First Total Synthesis of Cytotoxic Diarylheptanoids,Galeon,and Pterocarine

Qian Wang; Jong-Keun Son; Yurngdong Jahng

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First Total Synthesis of Cytotoxic Diarylheptanoids,Galeon,and Pterocarine

机译：首次全面合成细胞毒性二芳基庚烷，加仑和蝶草碱

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The first total synthesis of cytotoxic diphenyl ether-type diarylheptanoids,galeon and pterocarine,was described in which the Ullmann reaction was employed at the final step for the diaryl ether formation of key intermediate,l-(3-bromo-4-ben-zyloxyphenyl)-7-(4-hydroxy-3-methoxyphenyl)heptan-3-one,assembled by a series of cross-aldol condensation from 3-methoxy-4-benzyloxybenzaldehyde.

机译：描述了细胞毒性二苯醚型二芳基庚烷，加仑和蝶草碱的第一个全合成，其中在最后步骤中采用Ullmann反应形成关键中间体1-（3-溴-4-苯甲氧基苯）的二芳基醚）-7-（4-羟基-3-甲氧基苯基）庚烷-3-酮，由3-甲氧基-4-苄氧基苯甲醛经一系列的羟醛缩合组装而成。

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来源
《Synthetic Communications》 |2007年第6期|共7页
作者
Qian Wang; Jong-Keun Son; Yurngdong Jahng;
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原文格式 PDF
正文语种 eng
中图分类有机化学;
关键词
aldol; cytotoxicity; diatrylheptanoid; galeon; pterocarine; Ullmann reaction;

机译：羟醛;细胞毒性;腹泻类庚烷;加仑;蝶呤碱;乌尔曼反应;

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1. First Total Synthesis of Cytotoxic Diarylheptanoids,Galeon,and Pterocarine [J] . Qian Wang, Jong-Keun Son, Yurngdong Jahng Synthetic Communications . 2007,第4a6期

机译：首次全面合成细胞毒性二芳基庚烷，加仑和蝶草碱
2. Convergent total synthesis of (±) myricanol, a cyclic natural diarylheptanoid [J] . Bochicchio A., Schiavo L., Chiummiento L., Organic & biomolecular chemistry . 2018,第45期

机译：聚合全合成（±）肉豆蔻醇，一种环状天然二芳基庚烷
3. The first stereoselective total synthesis of a naturally occurring bioactive diarylheptanoid, (3R,6E)-1,7-bis(4-hydroxyphenyl)hept-6-en-3-ol, through two different approaches [J] . Kashanna J., Jangili P., Kumar R.A., Helvetica chimica acta . 2012,第9期

机译：天然存在的生物活性二芳基庚烷，（3R，6E）-1,7-双（4-羟苯基）庚-6-en-3-ol的首次立体选择性全合成，通过两种不同的方法
4. Progress toward the total synthesis of a cytotoxic norditerpene from Cephalotaxus sp. : the hainanolide (or harringtonolide)(Abstracts) [C] . Laurent Evanno, Bernard Bodo, Bastien Nay European Symposium on Organic Chemistry . 2007

机译：从头孢菌SP中朝着细胞毒性偏移的总合成的进展。：HainaNolide（或Harringtonolide）（摘要）
5. Total synthesis of microtubule stabilizing agent laulimalide and total syntheses of proposed structure of cytotoxic macrolide iriomoteolide-1a and -1b. [D] . Yuan, Hao. 2011

机译：微管稳定剂laulimalide的全合成和细胞毒性大环内酯iriomoteolide-1a和-1b拟议结构的总合成。
6. Natural Product Synthesis Special Feature: Total synthesis of the cytotoxic cyclodepsipeptide (-)-doliculide: The ester effect in acyclic 13-induction of deoxypropionates [O] . Stephen Hanessian, Vincent Mascitti, Simon Giroux 2004

机译：天然产物合成的特殊功能：细胞毒性环二肽（-）-doliculide的完全合成：无环13-脱氧丙酸酯的酯效应
7. Approaches to the total synthesis of a novel diarylheptanoid [O] . Vela Nomandla Magnificent 2008

机译：全新合成二芳基庚烷的方法

First Total Synthesis of Cytotoxic Diarylheptanoids,Galeon,and Pterocarine

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