A Cheap,Simple,and Versatile Method for Acetylation of Alcohols and Phenols and Selective Deprotection of Aromatic Acetates Under Solvent-Free Condition

Fatemeh Rajabi; Mohammad R.Saidi

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A Cheap,Simple,and Versatile Method for Acetylation of Alcohols and Phenols and Selective Deprotection of Aromatic Acetates Under Solvent-Free Condition

机译：一种廉价，简单和通用的无溶剂条件下的醇和苯酚乙酰化和芳香乙酸选择性脱保护的方法

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摘要

Acyclic and cyclic acetates of various alcohols and phenols were obtained in excellent yields under mild reaction conditions in the presence of a catalytic amount of sodium hydroxide under solvent-free conditions and microwave irradiation.Selective deprotection of acetate group from the corresponding phenolic compounds was carried out in the presence of LiClO_4 centre dot 2H_2O.

机译：在催化量的氢氧化钠存在下，在无溶剂条件下和微波辐射下，在温和的反应条件下以优异的收率获得了各种醇和酚的无环和环状乙酸酯，并从相应的酚类化合物中选择性地脱保护了乙酸酯基团。在LiClO_4中心点2H_2O的存在下。

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《Synthetic Communications》 |2005年第3期|共9页
作者
Fatemeh Rajabi; Mohammad R.Saidi;
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原文格式 PDF
正文语种 eng
中图分类有机化学;
关键词
Acetylation; alcohols; phenols; deprotection; solvent-free;

机译：乙酰化;醇;酚;脱保护;无溶剂;

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1. A Cheap,Simple,and Versatile Method for Acetylation of Alcohols and Phenols and Selective Deprotection of Aromatic Acetates Under Solvent-Free Condition [J] . Fatemeh Rajabi, Mohammad R.Saidi Synthetic Communications . 2005,第3期

机译：一种廉价，简单和通用的无溶剂条件下的醇和苯酚乙酰化和芳香乙酸选择性脱保护的方法
2. Simple and Efficient Method for Acetylation of Alcohols, Phenols, Amines, and Thiols Using Anhydrous NiCl₂ Under Solvent-Free Conditions [J] . Synthetic Communications . 2009,第24期

机译：无溶剂条件下使用无水NiCl _{2 的醇，苯酚，胺和硫醇乙酰化的简单有效方法}
3. Simple and Efficient Method for Acetylation of Alcohols, Phenols, Amines, and Thiols Using Anhydrous NiCl₂ Under Solvent-Free Conditions [J] . Synthetic Communications . 2009,第14期

机译：无溶剂条件下使用无水NiCl _{2 的醇，苯酚，胺和硫醇乙酰化的简单有效方法}
4. Nano-Fe3O4 as a New Reusable Catalyst for the Selective Acetylation of Alcohols and Phenols under Solvent Free Conditions [C] . Mohamad Zaman Kassaee, Monireh Ghavami 2011 2nd International Conference on Chemistry and Chemical Engineering . 2011

机译：纳米Fe3O4作为无溶剂条件下醇和苯酚选择性乙酰化的新型可重复使用催化剂
5. New developments toward the synthesis of heterocycles and applications in green chemistry. I. A simple and essentially one-pot synthesis of N-aminated heterocycles using phase transfer catalyst (Aliquat-336). II. Synthesis of pharmaceutically important pyrrole derivatives. III. Applications in green chemistry: Surfactant-mediated environmentally friendly cleavage of aromatic esters and trans-esterification under solvent-free neutral conditions . [D] . Patel, Nitinchandra. 2005

机译：杂环合成的新进展及其在绿色化学中的应用。 I.使用相转移催化剂（Aliquat-336）简单且基本上一锅合成N-胺化的杂环。二。药学上重要的吡咯衍生物的合成。三，在绿色化学中的应用：在无溶剂的中性条件下，表面活性剂介导的环境友好的芳族酯裂解和酯交换反应。
6. ZSM-5-SO3H: An Efficient Catalyst for Acylation of Sulfonamides Amines Alcohols and Phenols under Solvent-Free Conditions [O] . Ahmad Reza Massah, Roozbeh Javad Kalbasi, Mahdiehsadat Khalifesoltani, 2013

机译：ZSM-5-SO3H：无溶剂条件下磺酰胺类胺醇和苯酚酰化的高效催化剂
7. HIGHLY EFFICIENT AND VERSATILE ACETYLATION OF ALCOHOLS, PHENOLS AND AMINES CATALYZED BY METHYLENEDIPHOSPHONIC ACID (MDP) UNDER SOLVENT-FREE CONDITIONS [O] . MINHAO XIE, HONGYONG WANG, JUN WU, 2011

机译：在无溶剂条件下高效和通过亚甲基膦酸（MDP）催化的醇，酚和胺的高效和多功能乙酰化

A Cheap,Simple,and Versatile Method for Acetylation of Alcohols and Phenols and Selective Deprotection of Aromatic Acetates Under Solvent-Free Condition

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