N-linked hydroxylamine resin: Solid-phase synthesis of hydroxamic acids

Yin Z; Low K; Lye P

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N-linked hydroxylamine resin: Solid-phase synthesis of hydroxamic acids

机译：N-连接的羟胺树脂：异羟肟酸的固相合成

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摘要

A novel hydroxylamine resin for solid-phase synthesis of hydroxamic acids is described. Its facile application is illustrated by the solid-phase synthesis of various hydroxamic acids. Cleavage is induced under acidic conditions by treatment with trifluoroacetic acid, providing hydroxamic acids in high purity and good yields.

机译：描述了用于固相合成异羟肟酸的新型羟胺树脂。各种异羟肟酸的固相合成说明了其简便的应用。通过在酸性条件下用三氟乙酸处理诱导裂解，从而以高纯度和高收率提供异羟肟酸。

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《Synthetic Communications》 |2005年第23期|共6页
作者
Yin Z; Low K; Lye P;
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原文格式 PDF
正文语种 eng
中图分类有机化学;
关键词
hydroxamic acids; hydroxylamine resin; solid-phase synthesis; LINKAGE;

机译：异羟肟酸;羟胺树脂;固相合成;键合;

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专利

1. N-linked hydroxylamine resin: Solid-phase synthesis of hydroxamic acids [J] . Yin Z, Low K, Lye P Synthetic Communications . 2005,第23期

机译：N-连接的羟胺树脂：异羟肟酸的固相合成
2. One-Pot Synthesis of Hydroxamic Acids from Aldehydes and Hydroxylamine [J] . Giovanna Dettori, Silvia Gaspa, Andrea Porcheddu Advanced synthesis & catalysis . 2014,第11a12期

机译：由醛和羟胺一锅法合成异羟肟酸
3. Convenient Preparation of O-Linked Polymer-Bound N-Substituted Hydroxylamines, Intermediates for Synthesis of N-Substituted Hydroxamic Acids [J] . Dale E. Robinson, Mark W. Holladay Organic letters . 2000,第18期

机译：方便制备O-连接的聚合物结合的N-取代的羟胺，用于合成N-取代的羟肟酸的中间体
4. Solid-Phase Synthesis of N-Linked Glycans [C] . International symposium on fine chemistry and functional polymers . 2008

机译：N-连接聚糖的固相合成
5. The synthesis of enantiopure N-benzylidene nitrone α-amino acids for the preparation of N-terminal hydroxylamine peptides for chemoselective decarboxylative ligation with α-ketoacid peptides [D] . Medina, S. Irene 2011

机译：对映体纯N-亚苄基硝酮α-氨基酸的合成，用于制备N-端羟胺肽，用于与α-酮酸肽进行化学选择性脱羧连接
6. Convenient Synthesis of a Library of Discrete Hydroxamic Acids Using the Hydroxythiophenol (Marshall) Resin [O] . Jinil Choi, Jewn Giew Park, Yuan-Ping Pang -1

机译：使用羟基硫酚（马歇尔）树脂方便地合成离散的异羟肟酸库
7. Development of a UV-Cleavable Protecting Group for Hydroxylamines, Synthesis of a StructurallyWide Variety of Hydroxamic Acids, and Identification of Histone Deacetylase Inhibitors [O] . Mortensen Kim Thollund, Qvortrup Katrine, Nielsen Thomas Eiland 2017

机译：开发紫外线可裂解的羟胺保护基团，合成结构多种的异羟肟酸，并鉴定组蛋白去乙酰化酶抑制剂
8. Chelating Ion Exchange with Macroreticular Hydroxamic Acid Resins [R] . Phillips, R. J. 1980

机译：螯合离子交换与大网状异羟肟酸树脂

N-linked hydroxylamine resin: Solid-phase synthesis of hydroxamic acids

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