One-pot synthesis of salicylanilides by direct amide bond formation from salicyclic acid under microwave irradiation

Lu C.-R.; Zhao B.; Jiang Y.-P.; Ding H.; Yang S.

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One-pot synthesis of salicylanilides by direct amide bond formation from salicyclic acid under microwave irradiation

机译：微波辐射下水杨酸直接酰胺键一锅法合成水杨酰苯胺

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摘要

A highly efficient protocol for the preparation of aromatic amides is described by the direct reactions between salicyclic acid and aromatic amines in the presence of phosphorous trichloride under microwave irradiation. The method has several advantages over the conventional methods, including operational simplicity, good yield, and reduced reaction time.

机译：在微波辐射下，在三氯化磷存在下，水杨酸与芳族胺之间的直接反应描述了制备芳族酰胺的高效方法。与常规方法相比，该方法具有多个优点，包括操作简单，产率高以及反应时间缩短。

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《Synthetic Communications》 |2011年第9期|共10页
作者
Lu C.-R.; Zhao B.; Jiang Y.-P.; Ding H.; Yang S.;
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正文语种 eng
中图分类有机化学;
关键词
Microwave irradiation; salicylanilide; synthesis;

机译：微波辐射;水杨酰苯胺;合成;

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专利

1. One-pot synthesis of salicylanilides by direct amide bond formation from salicyclic acid under microwave irradiation [J] . Lu C.-R., Zhao B., Jiang Y.-P., Synthetic Communications . 2011,第7a9期

机译：微波辐射下水杨酸直接酰胺键一锅法合成水杨酰苯胺
2. Organic synthesis in solid media. Alumina supported sodium hydrogen sulfate as an effective and reusable catalyst for 'one-pot' synthesis of amides from ketones in dry media under microwave irradiation [J] . Gopalakrishnan M, Sureshkumar P, Kanagarajan V, Letters in organic chemistry . 2005,第5期

机译：固体介质中的有机合成。氧化铝负载的硫酸氢钠是一种有效和可重复使用的催化剂，用于微波辐射下在干燥介质中从酮“一锅”合成酰胺
3. Instability of Amide Bond with Trifluoroacetic Acid (20%): Synthesis, Conformational Analysis, and Mechanistic Insights into Cleavable Amide Bond Comprising β-Troponylhydrazino Acid [J] . Nihar Ranjan Dalabehera, Sagarika Meher, Bibhuti Bhusana Palai, ACS Omega . 2020,第40期

机译：与三氟乙酸（20％）的酰胺键的不稳定性：合成，构象分析和机械洞察分解酰胺键，其包含β-浓甲基酰肼基甲酸
4. One-Pot Amide Synthesis via Thermal Decomposition N-Acylureas under Microwave Irradiation [C] . N.S. Soldatova, K.V. Orlova, T.A. Sarycheva International Conference for Young Scientists "High Technology: Research and Applications" . 2016

机译：通过热分解N-酰基在微波辐射下合成单壶酰胺合成
5. 1. Reduction of Tertiary Benzamides to Benzaldehydes by an in situ-Generated Schwartz Reagent (Cp2 Zirconium (Hydrogen)Chloride); Formal Synthesis of Lysergic Acid. 2. Ru-Catalyzed Amide-Directed Aryl Carbon-Hydrogen, Carbon-Nitrogen and Carbon-Oxygen Bond Functionalizations: C-B Formation, Carbon-Carbon Suzuki Cross Coupling and Hydrodemethoxylation [D] . Zhao, Yigang 2011

机译：1.通过原位生成的Schwartz试剂（Cp2氯化锆（氢）氯化物）将叔苄酰胺还原为苯甲醛；麦角酸的正式合成。 2. Ru催化的酰胺基芳烃碳氢，碳氮和碳氧键功能化：C-B形成，碳-碳铃木交叉偶联和加氢脱甲氧基化
6. Instability of Amide Bondwith Trifluoroacetic Acid(20): Synthesis Conformational Analysis and Mechanistic Insightsinto Cleavable Amide Bond Comprising β-TroponylhydrazinoAcid [O] . NiharRanjan Dalabehera, §, Sagarika Meher, 2020

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7. Instability of Amide Bond with Trifluoroacetic Acid (20): Synthesis, Conformational Analysis, and Mechanistic Insights into Cleavable Amide Bond Comprising Troponylhydrazino Acid [O] . -1

机译：与三氟乙酸（20％）的酰胺键的不稳定性：合成，构象分析和机械洞察力酰胺酰胺粘合剂，其包含浓缩甲基酰基苯甲酸酯

One-pot synthesis of salicylanilides by direct amide bond formation from salicyclic acid under microwave irradiation

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