Conversion of Glycals to l-Azido-2-iodo Sugars Using N-Iodosuccinimide/Sodium Azide or Potassium Iodide/Oxone Reagent Systems: Application in the Synthesis of Methyl N-Acetyl-a-D-lividosaminide

Girish K. Rawal; Shikha Rani; K. P. Madhusudanan; Yashwant D. Vankar

首页> 外文期刊>Synthesis: International Journal of Methods in Synthetic Organic Chemistry >Conversion of Glycals to l-Azido-2-iodo Sugars Using N-Iodosuccinimide/Sodium Azide or Potassium Iodide/Oxone Reagent Systems: Application in the Synthesis of Methyl N-Acetyl-a-D-lividosaminide

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Conversion of Glycals to l-Azido-2-iodo Sugars Using N-Iodosuccinimide/Sodium Azide or Potassium Iodide/Oxone Reagent Systems: Application in the Synthesis of Methyl N-Acetyl-a-D-lividosaminide

机译：使用N-碘代琥珀酰亚胺/叠氮化钠或碘化钾/ Oxone试剂系统将乙二醇转化为L-叠氮基-2-碘糖：在甲基N-乙酰基-α-D-脂卫苷合成中的应用

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Abstract: Glycals are readily converted into the corresponding 2-deoxy-2-iodoglycosyl azides, in good to excellent yields in a short time, upon treatment with N-iodosuccinimide/sodium azide orspo-tassium iodide/Oxone reagent systems. One of these l-azido-2-iodo sugars was converted into methyl N-acetyl-a-D-lividosaminide.

机译：摘要：经N-碘代琥珀酰亚胺/叠氮化钠或碘化钾-碘化钾/异戊二酮试剂体系处理后，糖类很容易在短时间内以良好的优异转化率转化为相应的2-deoxy-2-iodoglycosyl azide。这些1-叠氮基-2-碘代糖中的一种被转化为甲基N-乙酰基-α-D-卵磷脂。

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来源
《Synthesis: International Journal of Methods in Synthetic Organic Chemistry》 |2007年第2期|共5页
作者
Girish K. Rawal; Shikha Rani; K. P. Madhusudanan; Yashwant D. Vankar;
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原文格式 PDF
正文语种 eng
中图分类有机化学;
关键词
glycals; N-iodosuccinimide; sodium azide; potassium iodide; Oxone; l-azido-2-iodo sugar; methyl N-acetyl-a-D-lividos-aminide;

机译：乙二醇;N-碘琥珀酰亚胺;叠氮化钠;碘化钾;酮;1-叠氮基-2-碘糖;甲基N-乙酰基-α-D-丁烯二酰亚胺;

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1. Conversion of Glycals to l-Azido-2-iodo Sugars Using N-Iodosuccinimide/Sodium Azide or Potassium Iodide/Oxone Reagent Systems: Application in the Synthesis of Methyl N-Acetyl-a-D-lividosaminide [J] . Girish K. Rawal, Shikha Rani, K. P. Madhusudanan, Synthesis: International Journal of Methods in Synthetic Organic Chemistry . 2007,第2期

机译：使用N-碘代琥珀酰亚胺/叠氮化钠或碘化钾/ Oxone试剂系统将乙二醇转化为L-叠氮基-2-碘糖：在甲基N-乙酰基-α-D-脂卫苷合成中的应用
2. N-Halosuccinimide/AgNO_3-Efficient Reagent Systems for One-Step Synthesis of 2-Haloglycals from Glycals: Application in the Synthesis of 2C-Branched Sugars via Heck Coupling Reactions [J] . Suresh Dharuman, Yashwant D. Vankar Organic letters . 2014,第4期

机译：N-卤代琥珀酰亚胺/ AgNO_3-高效试剂系统，可从乙二醇一步合成2-卤代糖：在通过Heck偶联反应合成2C支链糖中的应用
3. One-Step TEMPO-Catalyzed and Water-Mediated Stereoselective Conversion of Glycals into 2-Azido-2-deoxysugars with a PIFA–Trimethylsilyl Azide Reagent System [J] . Ande Chennaiah, Yashwant D. Vankar Organic letters . 2018,第9期

机译：用PIFA-三甲基甲硅烷基叠氮化物系统将甘油的一步的速度催化和水介导的蛋白质的立体选择转化为2-氮杂-2-脱氧葡萄节
4. Self-Propagating High-Temperature Synthesis of Composite Nanopowder AlN-BN From Systems "Sodium Azide - Halides of Aluminum and Boron" [C] . Ljudmila Shiganova, George Bichurov, Irina Kerson International Conference for Young Scientists "High Technology: Research and Applications" . 2016

机译：从系统“铝和硼氮化钠 - 卤化物”的复合纳米粉末ALN-BN自蔓延的高温合成。
5. Reagent-Controlled Dehydrative Glycosylation for Synthesis of 2-Deoxy-β-Linked Sugars: Applications to Oligosaccharide Synthesis [D] . Lloyd, Dina 2018

机译：试剂控制的脱水糖基化反应用于2-脱氧-β-连接糖的合成：在寡糖合成中的应用
6. Systems Silver Iodide-Sodium Iodide and Silver Iodide-Potassium Iodide [O] . G. Burley, H. E. Kissinger 1960

机译：系统碘化银-碘化钠和碘化银-碘化钾
7. Trimethylsilylnitrate-Trimethylsilylazide: A Novel Reagent System for the Synthesis of 2-Deoxy Glycosyl Azides from Glycals. Application in the Synthesis of 2-Deoxy beta-N-glycopeptides [O] . -1

机译：三甲基甲硅烷硫酸甲硅烷醚 - 三甲基甲硅烷醚：一种用于合成来自族种的2-脱氧糖基叠氮化物的新型试剂系统。在合成2-脱氧β-N-糖肽的合成中的应用
8. TWO-PHASE CRITICAL FLOW WITH APPLICATION TO LIQUID-METAL SYSTEMS (Mercury, Cesium, Rubidium, Potassium, Sodium, and Lithium) [R] . Hans K. Fauske 1963

机译：应用于液态金属系统的两相临界流量（汞，铯，铷，钾，钠和锂）

Conversion of Glycals to l-Azido-2-iodo Sugars Using N-Iodosuccinimide/Sodium Azide or Potassium Iodide/Oxone Reagent Systems: Application in the Synthesis of Methyl N-Acetyl-a-D-lividosaminide

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