Synthesis and Structure of 2-Nitroxyethylsuccinylaminodiethylmalonate

Fedorov B. S.; Fadeev M. A.; Golovina N. I.; Dorokhov V. G.; Shilov G. V.; Utenyshev A. N.

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Synthesis and Structure of 2-Nitroxyethylsuccinylaminodiethylmalonate

机译：2-硝基氧乙基琥珀酰氨基二乙基丙二酸酯的合成与结构

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Interaction of hydroxymethylnitrodiethylmalonate with ammonia produced, in contrast to published data, the ammonium salt of nitrodiethylmalonate; catalytic reduction of this compound with hydrogen followed by treatment with the chloranhydride of the 2-nitroxyethyl ester of succinamic acid yielded 2-nitroxyethylsuccinylaminodiethylmalonate. The final structures of the ammonium salt of nitrodiethylmalonate and 2-nitroxyethylsuccinylaminodiethylmalonate were identified by x-ray diffraction analysis.

机译：与已公开的数据相反，羟甲基硝基二乙基丙二酸羟甲基与氨的相互作用产生了硝基二乙基丙二酸铵盐。用氢催化还原该化合物，然后用琥珀酸的2-硝基羟乙基酯的氯酐处理，得到2-硝基羟乙基琥珀酰氨基二乙基丙二酸酯。通过X射线衍射分析鉴定了丙二酸二乙二乙酯和2-硝基氧乙基丁二酰氨基二乙基丙二酸铵盐的最终结构。

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《Pharmaceutical Chemistry Journal》 |2015年第3期|共4页
作者
Fedorov B. S.; Fadeev M. A.; Golovina N. I.; Dorokhov V. G.; Shilov G. V.; Utenyshev A. N.;
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正文语种 eng
中图分类药学;
关键词
hydroxymethylnitrodiethylmalonate; reaction with ammonia; ammonium salt of nitrodiethylmalonate; reaction with the chloranhydride of the 2-nitroxyethyl ester of succinamic acid; 2-nitroxyethylsuccinylaminodiethylmalonate; crystalline structure; x-ray diffraction analysis;

机译：羟甲基硝基二乙基丙二酸;与氨反应;丙二酸二乙基铵的铵盐;与琥珀酸的2-硝基羟乙基酯的氯酐反应;2-硝基羟乙基琥珀酰氨基二乙基丙二酸酯;晶体结构;X射线衍射分析;

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Synthesis and Structure of 2-Nitroxyethylsuccinylaminodiethylmalonate

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