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首页> 外文期刊>Philosophical Magazine Letters >Thermally activated step motion observed by high-resolution electron microscopy at a (113) symmetric tilt grain-boundary in aluminium
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Thermally activated step motion observed by high-resolution electron microscopy at a (113) symmetric tilt grain-boundary in aluminium

机译:通过高分辨率电子显微镜在铝中的(113)对称倾斜晶界处观察到热激活的步进运动

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摘要

Grain-boundary migration is demonstrated to proceed by lateral propagation of a small step in a (113), [110] symmetric Al tilt grain-boundary. In-situ high-resolution (transmission) electron microscopy (HREM) at 523 K allowed the study of atomic-scale detail at video rates during the migration process. The grain-boundary translational states on both sides of the step are identical, which leads to a step dislocation. This defect can move laterally by a combination of climb and glide. Dynamic HREM images indicate considerable atomic agitation within the dislocation core. A detailed temporal analysis of the step movements shows small random displacements of the dislocation core.
机译:晶界迁移被证明是通过在(113)[110]对称的Al倾斜晶界中的一小步横向传播而进行的。 523 K的原位高分辨率(透射)电子显微镜(HREM)允许在迁移过程中以视频速率研究原子尺度的细节。台阶两侧的晶界平移状态相同,这导致台阶错位。该缺陷可以通过爬升和滑行的组合而横向移动。动态HREM图像表明位错核心内有大量原子搅动。阶跃运动的详细时间分析显示,位错核心的随机位移较小。

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