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Method for the Synthesis of Tetranitroglycoluril from Imidazo-[4,5-d]-imidazoles with Loss of Dinitrogen Oxide.

机译：从咪唑 - [4,5-d] - 咪唑合成四硝基甘油的方法，其中氧化二氮的损失。

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A new method for the preparation of tetranitroglycoluril (TNGU, Sorguyl) is described, in which imidazo-[4,5-d]-imidazoles are nitrated with the elimination of N2O to generate TNGU. This method of TNGU synthesis results in material that is less sensitive than material produced with alternative routes. Additionally, a new spherical morphology of TNGU is disclosed. This morphology exhibits an even higher resistance to external insult even than material synthesized with the new method.

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作者
Sherrill, W. M.; Johnson, E. C.; Banning, J. E.;
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年度 2014
页码 1-12
总页数 12
原文格式 PDF
正文语种 eng
中图分类工业技术;
关键词
IMIDAZOLES; NITRATION; NITROGEN OXIDES; SYNTHESIS(CHEMISTRY); MORPHOLOGY; TNGU(TETRANITROGLYCOLURIL); SORGUYL; IMIDAZO 4 5-D IMIDAZOLES; DINITROGEN OXIDES; SPHERICAL MORPHOLOGY;

机译：咪唑;硝化;氮氧化物;合成（化学）;形态学; TNGU（四硝基甘油）; sORGUYL;咪唑-4,5-D咪唑;二硝基氧化物;球形态;

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专利

1. A Method for the Synthesis of Tetranitroglycoluril from lmidazo-[4,5-d]-imidazoles with Loss of Dinitrogen Oxide [J] . William M. Sherrill, Eric C. Johnson, Joseph E. Banning Propellants, Explosives, Pyrotechnics . 2014,第5期

机译：一种由咪唑-[4,5-d]-咪唑合成的四硝基甘露醇的合成方法
2. Synthesis and anti-HIV evaluation of 2',3'-dideoxy imidazo- and nu-triazolo(4,5-d)pyridazine nucleosides. [J] . Bussolari JC, Panzica RP Bioorganic and medicinal chemistry . 1999,第11期

机译：2'，3'-二脱氧咪唑-和三-三唑并（4,5-d）哒嗪核苷的合成及抗HIV评估。
3. 2-(2-Furyl)-5,6-dihydro-l(3)H-acenaphtho[4,5-d]imidazole. Synthesis and Electrophilic Substitution Reactions [J] . E.V.Illenzeer, A. A. Aleksandrov, M. M. Elchaninov Russian Journal of Organic Chemistry . 2012,第7期

机译：2-（2-呋喃基）-5，6-二氢-1（3）H-ac [4,5-d]咪唑。合成和亲电取代反应
4. cis-1,3,4,6-Tetranitrooctahydroimidazo-4,5-d imidazole (BCHMX) as a part of explosive mixtures [C] . Svatopluk Zeman, Ahmed K.Hussein, Ahmed Elbeih, International conference on defence technology . 2018

机译：CIS-1,3,4,6-四硝基乙二醇羟基咪唑-4,5-D咪唑（BCHMX）作为爆炸性混合物的一部分
5. Synthesis of pyrogallol and efforts in the synthesis of substituted imidazoles. [D] . Teli, Manoj Kumar. 2013

机译：邻苯三酚的合成和取代咪唑的合成。
6. Synthesis of Imidazole-Based Medicinal Molecules Utilizing the van Leusen Imidazole Synthesis [O] . Xunan Zheng, Zhengning Ma, Dawei Zhang 2020

机译：利用van Leusen咪唑合成法合成基于咪唑的药用分子
7. Synthesis and structure of new imidazo- and pyrazolo[5,1-d][1,2,3,5] thiatriazines based on the reaction of diazoazoles with acyl isothiocyanates controlled by Sa⋯O interaction [O] . Sadchikova, E. V., Bakulev, V. A., Subbotina, J. O., 2013

机译：基于重氮唑与Sa⋯O相互作用控制的酰基异硫氰酸酯反应合成新型咪唑并吡唑并[5,1-d] [1,2,3,5]噻三嗪

Method for the Synthesis of Tetranitroglycoluril from Imidazo-[4,5-d]-imidazoles with Loss of Dinitrogen Oxide.

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