• 主题
高级搜索  >
历史搜索 清空历史
首页> 美国政府科技报告 >Stability of Extractable Organic Constituents in Stored Samples of Gasification Condensates Inferred from Comparisons of GC/MS Total Ion Chromatograms
【24h】

Stability of Extractable Organic Constituents in Stored Samples of Gasification Condensates Inferred from Comparisons of GC/MS Total Ion Chromatograms

机译：GC / ms总离子色谱图比较推断气化凝析物储存样品中可萃取有机成分的稳定性

获取原文
页面导航
  • 摘要
  • 著录项
  • 相似文献
  • 相关主题

摘要

Samples of water and recycle oil were collected from the prequench tower of the gasifier crude-gas quench system of the HYGAS pilot plant. The samples were stored at refrigerator temperature (2-4 exp 0 C) for 60 days and at incubator temperature (37 exp 0 C) for 7 days. A dried oil sample and neutral, acid, base, and composite extracts were prepared at days 0, 29, and 60 for the refrigerated samples and at day 7 for the incubated sample. The extracts and dried oil were analyzed by capillary column gas chromatography/mass spectrometry on a 50-m OV-101 column. Minor differences in comparative total ion chromatogram traces can be attributed to variations in the concentrations of extraneous plasticizers or to slight differences in column resolution or sample extraction. No significant changes were apparent in comparative chromatogram traces for the refrigerated and incubated sample extracts and the dried oil. Within the limitations of this study, no degradation of organic components was found in the samples refrigerated for 60 days or in the sample stored at incubator temperature for 7 days. Argonne National Laboratory procedures for check-in, coding, and transfer of samples are also described. (ERA citation 04:035502)

著录项

相似文献

  • 外文文献
  • 中文文献
  • 专利
获取原文

客服邮箱：kefu@zhangqiaokeyan.com

京公网安备：11010802029741号 ICP备案号：京ICP备15016152号-6 六维联合信息科技 (北京) 有限公司©版权所有

  • 客服微信

  • 服务号