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X-RAY DIFFRACTOMETRY TECHNIQUES FOR CERAMIC FUELS

机译:陶瓷燃料的X射线衍射仪技术

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摘要

The design of suitable diffractometer-sample contain¬ment involving a nitrogen/argon two-gas system is described. Various mounting techniques are discussed and their relative merits are outlined.n.It was found that a resin mounting technique was most suitable for diffraction line profile measurements when (U Pu)02 was being examined. Analysis of small amounts of sesquicarbide and oxide phases in (U Pu)C was carried out using a paraffin wax binder followed by low-pressure pellet¬ing.

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