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A process for the low-temperature separation of air and air separation plant

机译:空分装置和空分装置的低温分离方法

摘要

It is a process for the low-temperature separation of air with the use of an air separation plant (100) with a distillation columns system (9, 12), the one on a first pressure level operated first high-pressure column (10) and a on a second pressure level operated second high-pressure column (11) as well as a on a third pressure level operated low-pressure column (9) and a on a fourth pressure level operated mixing column (7) has a. The first pressure level is at least 0,5 bar above the second pressure level, the third pressure level at least 2 bar below the second pressure level and the fourth pressure level differs by not more than 0,5 bar of the second or from the first pressure level. In the first high-pressure column (10) and in the second high-pressure column (11) are in each case gaseous compressed air flows (e, f), and this is fed in each case, liquid, oxygen-enriched bottom products and gaseous, nitrogen-enriched formed head product. From the low-pressure column (9), a liquid, an oxygen-rich current (o) is drawn off and, in the mixing column (7) the flow of compressed air fed in gaseous form (g) is sent, as a result of which is in the mixing column (7) a liquid bottom product and a gaseous top product form. The top product of the second high-pressure column (10), at least partially as a nitrogen-enriched stream (h) drawn off, with the use of the bottom product of the mixing column is cooled, and then into the second high-pressure column (10) is fed back to. For the cooling of the nitrogen enriched (h) with the use of the bottom product of the mixing column is a falling-film condenser (13) is used, the geodetically above the mixing column (12) is arranged, and the evaporation chamber is operated on the third pressure level. A corresponding air separation unit (100) is likewise subject matter of the present invention.
机译:这是通过使用具有蒸馏塔系统(9、12)的空气分离装置(100)进行空气的低温分离的方法,该装置在第一压力水平下操作的第一高压塔(10)在第二压力水平下操作的第二高压塔(11)以及在第三压力水平下操作的低压塔(9)和在第四压力水平下操作的混合塔(7)具有a。第一压力水平比第二压力水平高至少0.5 bar,第三压力水平比第二压力水平低至少2 bar,第四压力水平与第二压力水平或第二压力水平相差不超过0.5 bar。第一压力水平。在第一高压塔(10)和第二高压塔(11)中分别有气态的压缩空气流(e,f),并且在每种情况下将液态的,富氧的底部产物送入气态,富氮成型头产品。从低压塔(9)抽出液体,富氧电流(o),并在混合塔(7)中以气态形式(g)输送压缩空气流,作为其结果是在混合塔(7)中形成液体底部产物和气态顶部产物形式。利用混合塔的塔底产物,将第二高压塔(10)的塔顶产物至少部分地作为富氮物流(h)抽出,然后冷却至第二塔压力塔(10)被送回。为了使用混合塔的底部产物冷却富氮(h),使用了降膜冷凝器(13),在大地测量位置上布置了混合塔(12),并设置了蒸发室在第三压力水平下运行。相应的空气分离单元(100)同样是本发明的主题。

著录项

  • 公开/公告号DE102015015684A1

    专利类型

  • 公开/公告日2016-07-21

    原文格式PDF

  • 申请/专利权人 LINDE AKTIENGESELLSCHAFT;

    申请/专利号DE20151015684

  • 发明设计人 TOBIAS LAUTENSCHLAGER;

    申请日2015-12-03

  • 分类号F25J3/04;B01D3/00;

  • 国家 DE

  • 入库时间 2022-08-21 14:09:33

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