首页> 外国专利> Deposition of thin layers such as multi-layer coatings, nanolayers, nanostructures and nanocomposites by laser deposition from target materials on a substrate surface, comprises dividing the target into segments with materials

Deposition of thin layers such as multi-layer coatings, nanolayers, nanostructures and nanocomposites by laser deposition from target materials on a substrate surface, comprises dividing the target into segments with materials

机译:通过从衬底表面上的靶材料进行激光沉积来沉积诸如多层涂层,纳米层,纳米结构和纳米复合材料之类的薄层,包括将靶分成具有材料的片段

摘要

The method for the deposition of thin layers such as multi-layer coatings, nanolayers, nanostructures and nanocomposites by laser deposition from target materials on a substrate surface, comprises dividing the target (5) into segments (17, 18) with materials having differing physical and/or chemical properties, and irradiating the individual segments of the target with a respective different radiation intensity by a controlled energetic distribution (29) of the focused laser energy via the laser beam cross-section (28), so that each target segment absorbs the quantity of laser energy. The method for the deposition of thin layers such as multi-layer coatings, nanolayers, nanostructures and nanocomposites by laser deposition from target materials on a substrate surface, comprises dividing the target (5) into segments (17, 18) with materials having differing physical and/or chemical properties, and irradiating the individual segments of the target with a respective different radiation intensity by a controlled energetic distribution (29) of the focused laser energy via the laser beam cross-section (28), so that each target segment absorbs the quantity of laser energy during the irradiation, where the laser energy is required to evaporate or desorb the target material present in the respective segment. The target is displaced in a smooth, gradual and variable rotation during the coating process. The target or individual segments are displaced in a translational motion. During the rotation of the target, the target and/or each segment is displaced in the translational motion. The substrate is displaced in rotation and/or in translational motion during the coating process. The target is divided into a segment made of organic material and a segment made of inorganic material, is divided in a combination of segments made of organic material, metal and ceramic, and is divided into segments made of alloy or composite. The energetic distribution of the focused laser energy is determined by several factors influencing at the area of the target, where the factors are laser beam energy density, wavelength, pulse duration, the number of laser pulses, laser pulse repetition rate, substrate-target distance and target orientation. During the coating process, inert gases, reactive gases or gas mixture are supplied. An injection material is injected continuously or in pulsed field synchronization of the repetition rate of the laser to the target during the coating process, is made of helium/argon gas and is used for the production of ceramic-metal nanocomposites. The segments are arranged inside the target, so that they vary their position synchronization of the laser pulses. The energy density of the laser beam is adjusted by a polarization filter before entering to the segmented target for regulating the fluency depending on the position of the filter to the axis of the laser beam by 0-100%. The polarization filter and/or the target carry out a translational, rotational and/or synchronized motion. The optical filter is divided into different segments adapted to the segments of the target. Independent claims are included for: (1) a device for the deposition of thin layers such as multi-layer coatings, nanolayers, nanostructures and nanocomposites by laser deposition from target materials on a substrate surface; and (2) a substrate with a coating composition of organic-inorganic hybrid nanocomposites for the medical and pharmaceutical use.
机译:通过从衬底表面上的靶材料进行激光沉积来沉积诸如多层涂层,纳米层,纳米结构和纳米复合材料之类的薄层的方法,包括用具有不同物理性质的材料将靶(5)分成段(17、18)。和/或化学性质,并通过激光束横截面(28)通过聚焦激光能量的受控高能分布(29)用各自不同的辐射强度照射目标的各个片段,以使每个目标片段吸收激光能量的数量。通过从衬底表面上的靶材料进行激光沉积来沉积诸如多层涂层,纳米层,纳米结构和纳米复合材料之类的薄层的方法,包括用具有不同物理性质的材料将靶(5)分成段(17、18)。和/或化学性质,并通过激光束横截面(28)通过聚焦激光能量的受控高能分布(29)用各自不同的辐射强度照射目标的各个片段,以使每个目标片段吸收辐照期间的激光能量,其中需要激光能量来蒸发或解吸存在于各个段中的目标材料。在涂覆过程中,目标以平滑,渐变和可变的旋转方式移动。目标或单个段以平移运动进行移位。在目标旋转期间,目标和/或每个节段在平移运动中移动。在涂覆过程中,基板旋转旋转和/或平移。将靶分为由有机材料制成的片段和由无机材料制成的片段,将其分为由有机材料,金属和陶瓷制成的片段的组合,并分为由合金或复合材料制成的片段。聚焦激光能量的能量分布由影响靶区域的几个因素决定,这些因素包括激光束能量密度,波长,脉冲持续时间,激光脉冲数,激光脉冲重复率,衬底到目标的距离和目标定位。在涂覆过程中,会提供惰性气体,反应性气体或混合气体。在涂覆过程中,将注入材料连续注入或以脉冲场同步方式将激光的重复速率注入靶材,该注入材料由氦/氩气制成,用于生产陶瓷-金属纳米复合材料。这些段被布置在目标内部,从而它们改变了激光脉冲的位置同步。激光束的能量密度在进入分段目标之前要通过偏振滤镜进行调节,以根据滤镜相对于激光束轴的位置将通量调整为0-100%。偏振滤光器和/或目标执行平移,旋转和/或同步运动。滤光器分为适合于目标物的部分的不同部分。包括以下独立权利要求:(1)一种用于通过从基板表面上的目标材料进行激光沉积来沉积诸如多层涂层,纳米层,纳米结构和纳米复合材料之类的薄层的装置; (2)具有用于医疗和制药用途的有机-无机杂化纳米复合材料的涂料组合物的基材。

著录项

  • 公开/公告号DE102009031768A1

    专利类型

  • 公开/公告日2011-01-13

    原文格式PDF

  • 申请/专利权人 VASCOTEC GMBH;

    申请/专利号DE20091031768

  • 发明设计人 HERBST FRANZ;SERBEZOV VALERY;

    申请日2009-06-30

  • 分类号C23C14/28;B82B3/00;

  • 国家 DE

  • 入库时间 2022-08-21 17:47:50

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