首页> 外国专利> A method for preparation of oryzanol powder oryzanol powder prepared thereby and a method for preventing oxidization of meat and meat products by addition of oryzanol powder thereto

A method for preparation of oryzanol powder oryzanol powder prepared thereby and a method for preventing oxidization of meat and meat products by addition of oryzanol powder thereto

机译:制备谷维素粉的方法,由此制备的谷维素粉,以及通过向其中添加谷维素粉防止肉和肉制品氧化的方法

摘要

PURPOSE: Provided are a method for preparation of oryzanol powder, the oryzanol powder prepared thereby and a method for preventing oxidization of meat and processed meat products by adding a natural antioxidant the oryzanol powder thereto, thereby extending self-life of the meat and the processed meat products. CONSTITUTION: The oryzanol powder is manufactured by the steps of: mixing rice bran and hexane in a mixing ratio of 1:2, and followed by stirring and filtering it to give an extract; heating the extract, adding NaOH solution thereto and cooling them at room temperature; leaving the solution to obtain precipitates by centrifugation then separating a solid alkali agent therefrom; mixing the separated solid alkali gent with distilled water in a mixing ratio of 1:10 and followed by dissolving the mixture and controlling its pH to 7-11; re-mixing the obtained alkali solution with methanol and diethyl ether then recovering a diethyl ether layer; adding 5% KOH to the recovered diethyl ether layer then separating KOH layer; removing water and the solvent from the remaining ether layer then concentrating it; separating and purifying oryzanol concentrate from the concentrate by column chromatography; and crystallizing the purified material and heat-drying crystals to obtain oryzanol powder.
机译:用途:提供一种制备谷维素粉的方法,由此制备的谷维素粉以及通过向其添加天然抗氧化剂谷维素粉而防止肉类和加工肉制品氧化的方法,从而延长了肉类和加工品的自寿命肉制品。组成:谷维素粉末的制备步骤是:将米糠和己烷以1:2的混合比混合,然后搅拌并过滤,得到提取物;加热提取物,向其中加入NaOH溶液,并在室温下冷却。离心分离溶液,得到沉淀物,然后从中分离出固体碱剂。以1:10的混合比将分离的固体碱试剂与蒸馏水混合,然后溶解混合物并将其pH控制为7-11;将获得的碱溶液与甲醇和乙醚重新混合,然后回收乙醚层。向回收的乙醚层中添加5%的KOH,然后分离KOH层;从剩余的醚层中除去水和溶剂,然后浓缩。通过柱色谱从浓缩物中分离和纯化谷维素浓缩物;使纯化的物质结晶并加热干燥晶体以获得谷维素粉末。

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