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A process for preparing a citrate ester a citrate ester prepared thereby and a polymer containing the same

机译:柠檬酸酯的制备方法,由此制备的柠檬酸酯和包含该柠檬酸酯的聚合物

摘要

Described are processes for producing citrate esters in, an economic fashion. Esters are prepared by esterification of a citric acid-containing fermentation broth having been treated to remove cations and optionally other impurities, but containing sugar(s). Esters are also prepared by reacting an impure aqueous citric acid source with an alcohol to provide a heterogeneous aqueous/organic reacted mixture, wherein the organic phase contains the ester and the aqueous phase retains water-soluble impurities. A liquid phase separation is then used to separate the organic and aqueous phases, conveniently separating the impurities from the product and avoiding the energy-intensive distillation of water from the reaction medium.
机译:描述了一种以经济方式生产柠檬酸酯的方法。通过将经过处理以除去阳离子和任选的其他杂质但含有糖的含柠檬酸的发酵液酯化来制备酯。还通过使不纯柠檬酸水源与醇反应以提供不均匀的水/有机反应混合物来制备酯,其中有机相包含酯,并且水相保留水溶性杂质。然后使用液相分离法分离有机相和水相,方便地从产物中分离出杂质,并避免了从反应介质中对水进行能量密集的蒸馏。

著录项

  • 公开/公告号IL132806D0

    专利类型

  • 公开/公告日2001-03-19

    原文格式PDF

  • 申请/专利权人 REILLY INDUSTRIES INC.;

    申请/专利号IL19980132806

  • 发明设计人

    申请日1998-05-12

  • 分类号7C07CA;

  • 国家 IL

  • 入库时间 2022-08-22 01:25:01

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