首页> 外文会议>International Symposium on Nanocomposites and Nanoporous Materials;ISNAM; 20060215-17;20060215-17; Gyeongju(KR);Gyeongju(KR) >Characterization of Nano Scaled Mullite Powders Prepared by Organic-Inorganic Solution Technique
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Characterization of Nano Scaled Mullite Powders Prepared by Organic-Inorganic Solution Technique

机译:有机-无机溶液技术制备的纳米级莫来石粉的表征

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Nano scaled mullite (3Al_2O_3·2SiO_2) powders had been fabricated by an organic-inorganic solution technique using a polyvinyl alcohol (PVA) as an organic carrier. PVA polymer contributed to a soft and porous powder microstructure, and ball milling with the porous powder was effective in making nano-sized mullite powders. In addition, the degree of polymerization of PVA affected the crystallization behavior. The fully crystallized and ball-milled mullite powders had an average particle size of 120 nm with a specific surface area of 67.0 m~2/g. In this paper, the simple solution technique and milling process for the fabrication of nano scaled mullite powders are introduced. And the effects of PVA on the crystallization behavior and powder specific surface area are also studied. The characteristics of the synthesized powders are examined by using XRD, TEM, particle size analyzer and nitrogen gas adsorption.
机译:利用聚乙烯醇(PVA)作为有机载体,通过有机-无机溶液技术制备了纳米级莫来石(3Al_2O_3·2SiO_2)粉末。 PVA聚合物有助于形成柔软且多孔的粉末微结构,用该多孔粉末进行球磨可有效制备纳米尺寸的莫来石粉末。另外,PVA的聚合度影响结晶行为。完全结晶和球磨的莫来石粉末具有120nm的平均粒径,比表面积为67.0m 2 / g。本文介绍了制备纳米级莫来石粉的简单方法和研磨工艺。并且研究了PVA对结晶行为和粉末比表面积的影响。使用XRD,TEM,粒度分析仪和氮气吸附对合成粉末的特性进行了检查。

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