Preparation and characterization of 3,5-diamino-1,2,4-triazolium 4,4',5,5'-tetranitro-2,2'-biimidazolate (DATNBI)

机译：3,5-二氨基-1,2,4-三唑鎓4,4'，5,5'-四硝基-2,2'-联咪唑啉酸酯（DATNBI）的制备和表征

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Ionic derivatives of 4,4',5,5'-tetranitro-2,2'-biimidazole (TNB1) are of growing interest to many researchers these days. Amongst the others, there is 3,5-diamino-1,2,4-triazolium 4,4',5,5'-tetranitro-2,2'-biimidazolate (DATNBI) The salt can be easily prepared from widely available substrates. After filtration and drying, it shows no signs of hygroscopicity and decomposes at 239 °C. The structure of obtained compound was confirmed with NMR spectroscopy and elemental analysis. Thermal properties were investigated with DTA/TG analysis. We also determined standard enthalpy of formation. Detonation parameters were calculated with CHEETAH code for density determined for pressed sample. Some of the energetic properties were measured experimentally.

机译：如今，4,4'，5,5'-四硝基-2,2'-联咪唑（TNB1）的离子衍生物已引起许多研究人员的关注。除其他外，还有3,5-二氨基-1,2,4-三唑鎓4,4'，5,5'-四硝基-2,2'-联咪唑酸盐（DATNBI）可以很容易地从广泛使用的底物上制备盐。过滤并干燥后，它没有显示出吸湿性的迹象，并在239°C时分解。所得化合物的结构通过NMR光谱法和元素分析确认。用DTA / TG分析研究热性能。我们还确定了标准的形成焓。用CHEETAH代码计算爆轰参数，确定压制样品的密度。一些能量性质是通过实验测量的。

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《Seminar on New Trends in Research of Energetic Materials》|2016年|735-739|共5页
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Rafal Lewczuk; Mateusz Szala; Judyta Recko;
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TNBI; energetic salts; synthesis;

机译：TNBI;高能盐合成;

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2. Preparation and characterization of nano N,N '-bis(1,2,4-triazol-3-yl-)-4,4 '-diamino-2,2 ', 3,3 ', 5,5 ', 6,6 '-octanitroazo-benzene explosive [J] . Mousavi S., Esmaeilpour K., Keshavarz M. H. Indian journal of engineering and materials sciences . 2014,第5期

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4. Preparation and characterization of 3,5-diamino-1,2,4-triazolium 4,4',5,5'-tetranitro-2,2'-biimidazolate (DATNBI) [C] . Rafal Lewczuk, Mateusz Szala, Judyta Recko Seminar on New Trends in Research of Energetic Materials . 2016

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5. Synthesis and characterization of novel platinum(II) and platinum(IV) complexes containing 4,4'-disubstituted-2,2'- bipyridine ligands for the treatment of cancer. [D] . Vo, Van. 2014

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机译：Bishydrazinium和二铵盐4,4'，5,5'-四硝基-2,2'-联咪唑（TNBI）：合成和性质。

Preparation and characterization of 3,5-diamino-1,2,4-triazolium 4,4',5,5'-tetranitro-2,2'-biimidazolate (DATNBI)

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