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Optical study of plasma sprayed hydroxyapatite coatings deposited at different spray distance

机译:等离子喷涂羟基磷灰石涂层在不同喷涂距离下的光学研究

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Series of hydroxyapatite (HA) coatings deposited on titanium substrate at different spray (plasma gun to workpiece) distance were investigated. The optical methods as dark field confocal microscopy, Raman/PL and UV-VIS spectroscopy were used for study the influence of deposition process on structural degradation of HA precursor. The hydroxyl group concentration was investigated by study the OH mode intensity in the Raman spectra. Optical absorption coefficients at near UV region were analyzed by Diffuse Reflectance Spectroscopy. PL intensity observed during Raman measurement was also considered as relation to defects concentration and degradation level. It was confirmed the different gun-substrate distance has a great impact on structure of deposited HA ceramics.
机译:研究了在不同喷涂距离(等离子枪到工件)距离下沉积在钛基体上的一系列羟基磷灰石(HA)涂层。利用暗场共聚焦显微镜,拉曼/ PL和紫外可见光谱等光学方法研究了沉积工艺对HA前驱体结构降解的影响。通过研究拉曼光谱中的OH模式强度来研究羟基浓度。通过漫反射光谱分析在近UV区域的光吸收系数。拉曼测量过程中观察到的PL强度也被认为与缺陷浓度和降解水平有关。证实了不同的枪-基片距离对沉积的HA陶瓷的结构有很大的影响。

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