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X-RAY POWDER DIFFRACTION ANALYSIS OF LIQUID-PHASE-SINTERED SILICON CARBIDE CERAMICS

机译:液相烧结碳化硅陶瓷X射线粉末衍射分析

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In an attempt to gain a comprehensive understanding of the microstructural evolution in liquid-phase-sintered silicon carbide ceramics, the effect of the starting β-SiC powder has been studied. Pellets of two different β-SiC starting powders were sintered with simultaneous additions of Al_2O_3 and Y_2O_3 at 1950°C for 1 hour in flowing argon atmosphere. Here we have used X-ray diffraction to obtain the relative abundance of the resulting SiC polytypes after sintering. The significant influence of the defects concentration on the β to α transformation rate has been determined using the Rietveld method.
机译:在尝试全面了解液相烧结碳化硅陶瓷中的微观结构演化,已经研究了起始β-SiC粉末的效果。两种不同的β-SiC起始粉末的颗粒在1950℃下同时加入Al_2O_3和Y_2O_3在流动的氩气氛中加入1小时。在这里,我们使用X射线衍射在烧结后获得所得SiC多型的相对丰度。使用RIETVELD方法确定了缺陷浓度对β至α转化率的显着影响。

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