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A green sample preparation method for the determination of chloramphenicol and its metabolite residues in meat and milk using ESI-LCMS/MS

机译：使用ESI-LCMS / MS测定肉和牛奶中氯霉素及其代谢物残留的绿色样品制备方法

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A simple and rapid method for the determination of chloramphenicol and its metabolite residues by DLLME/ESI-LC-MS/MS was developed. The developed and validated DLLME/ESI-LC-MS/MS method was applied to muscle and milk biological matrices. The LOD was between 0.08 and 3.31 μg/Kg and the LOQ were 0.63 6.84 respectively for chloramphenicol, thaimphenicol and florfenicol.

机译：通过DLLME / ESI-LC-MS / MS进行简单且快速地测定氯霉素及其代谢物残留方法。将开发和验证的DLLME / ESI-LC-MS / MS方法应用于肌肉和牛奶生物学基质。 LOD分别在0.08和3.31μg/ kg之间，氯霉素，Thaimphenicol和Florfenicol分别为0.63 6.84。

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《ASMS Conference on Mass Spectrometry and Allied Topics》|2016年|1CD|共1页
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Ompelege E. Kemokgatla; Simiso Dube; Mathew M. Nindi;
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中图分类 TB994.5-53;
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1. Determination of chloramphenicol residues in industrialized milk and honey samples using LC-MS/MS [J] . Applied Biosystems do Brasil Ltda S?o Paulo Brasil, Bustillos Oscar Vega, Instituto de Pesquisas Energéticas e Nucleares S?o Paulo Brasil, Quimica nova . 2006,第3期

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2. Determination of chloramphenicol residues in meat, seafood, egg, honey, milk, plasma and urine with liquid chromatography-tandem mass spectrometry, and the validation of the method based on 2002/657/EC [J] . Ronning HT, Einarsen K, Asp TN Journal of chromatography, A: Including electrophoresis and other separation methods . 2006,第2期

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4. A green sample preparation method for the determination of chloramphenicol and its metabolite residues in meat and milk using ESI-LCMS/MS [C] . Ompelege E. Kemokgatla, Simiso Dube, Mathew M. Nindi ASMS Conference on Mass Spectrometry and Allied Topics . 2016

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A green sample preparation method for the determination of chloramphenicol and its metabolite residues in meat and milk using ESI-LCMS/MS

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