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首页> 外文会议>International Conference on Environmental Science and Technology >( cest2017_00741) Synthesis of Mesoporous Silica-Alumina from Lapindo Mud Using Gelatin from Catfish Bone as a Template: Effect of Extracting Temperature on Yield and Characteristic of Gelatin as well as Mesoporous Silica-Alumina
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( cest2017_00741) Synthesis of Mesoporous Silica-Alumina from Lapindo Mud Using Gelatin from Catfish Bone as a Template: Effect of Extracting Temperature on Yield and Characteristic of Gelatin as well as Mesoporous Silica-Alumina

机译：（CEST2017_00741）使用从鲶鱼骨中的明胶从LAPINDO泥浆中合成介孔二氧化硅 - 氧化铝作为模板：提取温度对明胶的产量和特征以及中孔二氧化硅 - 氧化铝的影响

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摘要

Mesoporous silica-alumina was synthesized from silicaand alumina extracted from Lapindo mud with gelatinfrom catfish bone as a template. The bone was refluxed indemineralized water at 60, 70, 80 and 90 °C to extract thegelatin. Gelatin was analyzed by FTIR and SDS-PAGE.The alumina was separated from the mud by reflux methodusing HCl solution and the silica was separated form mudby reflux method using NaOH solution. The purity of silicaand alumina were determined by XRF. The mesoporoussilica-alumina was synthesized using SiO2 and Al2O3 fromLapindo mud and the catfish gelatin as a template underhydrothermal method at 100 °C for 24 h and calcined at 500°C for 5 h and characterized by TEM and N2 adsorptiondesorption.The yield of extracted gelatin at 60, 70, 80 and90 °C was 4.79%, 6.09%, 8.13% and 12.24.%, respectively.The purity of silica and alumina extracted from Lapindomud were 100% and 89.69%. The synthesized silicaaluminashowed mesoporous characters and had porediameter of 105.14 ?, pore volume of 0.1974 cc/g andBET surface area of 75.105 m2/g.
机译：中孔二氧化硅 - 氧化铝由从Lapindo泥浆中萃取的二氧化硅和氧化铝用明胶，从鲶鱼骨中作为模板。将骨在60,70,80和90℃下回流吲哚水，以提取酚素。通过FTIR和SDS-PAGE分析明胶。通过回流通过回流分离氧化铝，使用NaOH溶液分离二氧化硅，形成泥浆回流法。二氧化硅和氧化铝的纯度通过XRF测定。中孔酰胺 - 氧化铝使用SiO 2和Al 2 O 3从苜蓿泥浆和鲶鱼明胶作为模板在100℃下以100℃下的24小时合成，并在500℃下煅烧5小时，并通过TEM和N 2吸附剂表征。提取的明胶产率在60,70,80和90℃下为4.79％，6.09％，8.13％和12.24％。％，二氧化硅和氧化铝的纯度为100％和89.69％。合成的二氧化硅轮型型介孔特性，含有105.14的毛细胞表现，孔体积为0.1974cc / g腹部表面积为75.105m 2 / g。

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