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XRD, EDX and Thermal Analysis of Glycine Doped Ammonium Dihydrogen Phosphate Crystal

机译:XRD,EDX和甘氨酸掺杂铵二氢磷酸盐的热分析

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Glycine doped Ammonium Dihydrogen Phosphate (ADP) Crystals were grown in different molar concentrations. Addition of glycine has increased the quality of the crystal by yielding highly transparent crystals. The grown crystals were subjected to XRD, EDX and TGA-DTA studies. The powder XRD study was conducted to verify the single phase nature of the samples. The powder XRD results reveal that the obtained diffracted peaks are same as pure ADP crystal. All elements present in the sample were confirmed by their respective energy peak observed in the EDX spectrum. From DTA, it is observed that the decomposition temperature is decreased by the addition of glycine. The TGA curve for all the doped crystals exhibited negligible weight loss in the region 40°C to 200°C showing the thermal stability in this temperature range.
机译:甘氨酸掺杂的磷酸二氢铵(ADP)晶体以不同的摩尔浓度生长。通过产生高度透明的晶体,甘氨酸的添加增加了晶体的质量。将生长的晶体进行XRD,EDX和TGA-DTA研究。进行粉末XRD研究以验证样品的单相性质。粉末XRD结果表明,所获得的衍射峰与纯ADP晶体相同。通过在EDX光谱中观察到的各自的能量峰来证实样品中存在的所有元素。从DTA中,观察到通过添加甘氨酸来降低分解温度。所有掺杂晶体的TGA曲线在40℃至200℃下表现出可忽略的重量损失,显示该温度范围内的热稳定性。

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