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Study on the Preparation of WO_3/TiO_2 Composite Photocatalyst and its Photocatalytic Activity

机译:WO_3 / TiO_2复合光催化剂制备及其光催化活性研究

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WO_3/TiO_2 composite photocatalyst was prepared from tetrabutyl titanate, ammonium tungstate by sol-gel method. The influence of acetic acid and ethanol on the gel point time, and the influence of doping amount of W on the photocatalytic activity was studied. The properties of powders were characterized by Fourier transform infrared spectrometer (FT-IR), and the photocatalytic activity was characterized by probe reaction of methyl orange degradation. The results show that the homogeneous transparent precursor is prepared at the amount of acetic acid =1mL and the amount of ethanol =10mL. When the doping amount of W reached to 0.12%, the best photocatalysis efficiency was obtained. Under the experimental conditions, the infrared absorption band of the W-O was not observed.
机译:通过溶胶 - 凝胶法制备钛酸四丁酯,钨酸盐铵制备WO_3 / TiO_2复合光催化剂。研究了乙酸和乙醇对凝胶点时间的影响,以及W对光催化活性的掺杂量的影响。通过傅里叶变换红外光谱仪(FT-IR)的特征在于粉末的性质,并通过析甲基橙降解的探针反应来表征光催化活性。结果表明,均匀透明前体以乙酸的量制备= 1mL,乙醇量= 10ml。当掺杂量的W达到0.12%时,获得最佳的光催化效率。在实验条件下,未观察到W-O的红外吸收带。

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