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Validation of Ion Chromatographic Method for Determination of Standard Inorganic Anions in Treated and Untreated Drinking Water

机译:离子色谱法测定治疗和未处理饮用水中标准无机阴离子的离子色谱法

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An ion chromatographic method for determination of fluoride, chloride, nitrate and sulphate in untreated and treated drinking waters was described. An automated 850 IC Professional, Metrohm system equipped with conductivity detector and Metrosep A Supp 7-250 (250 x 4 mm) column was used. The validation of the method was performed for simultaneous determination of all studied analytes and the results have showed that the validated method fits the requirements of the current water legislation. The main analytical characteristics were estimated for each of studied analytes: limits of detection, limits of quantification, working and linear ranges, repeatability and intermediate precision, recovery. The trueness of the method was estimated by analysis of certified reference material for soft drinking water. Recovery test was performed on spiked drinking water samples. An uncertainty was estimated. The method was applied for analysis of drinking waters before and after chlorination.
机译:描述了用于测定未处理和处理的饮用水中氟化物,氯化物,硝酸盐和硫酸盐的离子色谱法。使用自动化850 IC专业,配备电导率检测器和MetroSEP ACCUP 7-250(250×4mm)柱的Metrohm系统。对该方法的验证进行了用于同时测定所有研究的分析物,结果表明,验证的方法符合当前水立法的要求。估计研究的每个分析物的主要分析特征:检测限,定量限制,工作和线性范围,可重复性和中间精度,恢复。通过对软饮水认证参考材料的分析估算了该方法的真实性。在尖刺的饮用水样品上进行恢复试验。估计不确定性。该方法用于分析氯化前后饮水水。

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