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Preparation of Mixed Molecularly Imprinted Polymer Magnetic Nanoparticles and Its Application in Separation of Chinese Traditional Medicine

机译:混合分子印迹聚合物磁性纳米粒子的制备及其在中药分离中的应用

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A mixed imprinted polymer which can rapidly adsorb all flavonoids from raspberry extract was prepared and recycled. The hybrid molecular surface imprinted polymers were prepared by using quercetin as the template molecule and Fe_3O_4 magnetic nanospheres as the carrier. The molecular imprinting polymer was prepared by using the "initial template molecule, molecularly imprinted polymer, mixed template molecule, molecularly imprint ted polymers (MIPS)". The adsorption performance and durability of the hybrid molecularly imprinted polymers were investigated by using the fingerprints of the ethyl acetate fraction of raspberry as an index. The adsorption of flavonoids from raspberry extract, lindenoside, cis-lindenin, quercetin, kaempferol and other flavonoids was completely adsorbed by mixed molecular-imprinted polymer, and the other components were basically adsorbed. When Mix-IMPs were repeatedly used 10 times, the fingerprints showed that the content and content of flavonoids were basically the same. The experimental results show that Mix-IMPs has good adsorption performance, can be recycled and used for rapid enrichment of flavonoids in raspberry.
机译:制备可以快速吸附来自覆盆子提取物的所有类黄酮的混合印迹聚合物并再循环。通过使用槲皮素作为模板分子和Fe_3O_4磁性纳米球作为载体制备杂种分子表面压印的聚合物。通过使用“初始模板分子,分子印迹聚合物,混合模板分子,分子压印纹理聚合物(MIPS)”制备分子印迹聚合物。通过使用覆盆子的乙酸乙酯级分的指纹作为指数,研究了杂种分子印迹聚合物的吸附性能和耐久性。通过混合分子印迹聚合物完全吸附来自覆盆子提取物,林纳苷,顺式 - 林丁蛋白,槲皮素,kaempferol和其他类黄酮的黄酮类化合物的吸附,并且基本上吸附了其他组分。当重复使用混合偶尔10次时,指纹表明黄酮类化合物的含量和含量基本相同。实验结果表明,混合物具有良好的吸附性能,可以再循环并用于快速富集覆盆子中的黄酮类化合物。

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