• 主题
高级搜索  >
历史搜索 清空历史
首页> 外文会议>Proceedings of the workshop on knudsen effusion mass spectrometry >The Design, Construction, and Testing of a Knudsen Effusion Mass Spectrometric System Suitable for Studies of Nuclear Fuel Materials
【24h】

The Design, Construction, and Testing of a Knudsen Effusion Mass Spectrometric System Suitable for Studies of Nuclear Fuel Materials

机译：适用于核燃料材料研究的Knudsen扩散质谱系统的设计，构建和测试

获取原文
获取原文并翻译 | 示例
页面导航
  • 摘要
  • 著录项
  • 相似文献
  • 相关主题

摘要

Benefiting hugely from many years of experience of conducting vaporization studies with a commercially bought magnetic sector instrument (VG Micromass 30 BK), we designed and constructed a KEMS system having a quadrupole mass spectrometer. It essentially consisted of two chambers, one housing the Knudsen cell furnace assembly and the other housing the QMS with an indigenously designed and fabricated vacuum-isolation valve between these two chambers. The QMS initially used was from Extrel, but later that from Hiden was installed. Systematic vaporization experiments were undertaken on iron, nickel, chromium, zirconium, a Fe-Al alloy, MnO, uranium, and a U-Zr alloy. Electron bombardment heating was employed and the temperatures were measured by sighting the optical pyrometer onto a blackbody hole drilled at the bottom of the Knudsen cell. The results on the elements and the Fe-Al alloy were satisfactory while those on MnO, U, and U-Zr alloy were disconcerting but interesting and educative.
机译：得益于多年使用商业购买的磁性扇区仪器（VG Micromass 30 BK）进行汽化研究的经验，我们设计并构建了具有四极质谱仪的KEMS系统。它主要由两个腔室组成，一个腔室容纳Knudsen电池炉组件，另一个腔室容纳QMS，在这两个腔室之间具有本地设计和制造的真空隔离阀。最初使用的QMS来自Extrel，但后来安装了Hiden的QMS。在铁，镍，铬，锆，Fe-Al合金，MnO，铀和U-Zr合金上进行了系统汽化实验。使用电子轰击加热，通过将光学高温计对准在Knudsen池底部钻的黑体孔上来测量温度。元素和Fe-Al合金的结果令人满意，而MnO，U和U-Zr合金的结果令人不安，但有趣且具有教育意义。

著录项

  • 来源
  • 会议地点 Julich(DE)
  • 作者

    D. Darwin Albert Raj; R. Viswanathan; P. Manikandan;

  • 作者单位

    Fuel Chemistry Division, Chemistry Group, Indira Gandhi Centre for Atomic Research,Kalpakkam, Tamil Nadu 603102, India;

    Fuel Chemistry Division, Chemistry Group, Indira Gandhi Centre for Atomic Research,Kalpakkam, Tamil Nadu 603102, India;

    Fuel Chemistry Division, Chemistry Group, Indira Gandhi Centre for Atomic Research,Kalpakkam, Tamil Nadu 603102, India;

  • 会议组织
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

相似文献

  • 外文文献
  • 中文文献
  • 专利
获取原文

客服邮箱：kefu@zhangqiaokeyan.com

京公网安备：11010802029741号 ICP备案号：京ICP备15016152号-6 六维联合信息科技 (北京) 有限公司©版权所有

  • 客服微信

  • 服务号