A method was developed for determination of 17 phthalate esters residues in drinks using QuEChERS and gas chromatography-tandem mass spectrometry (GC/MS/MS). The samples were extracted with n-hexane and cleaned up with dispersive-solid phase extraction. The extracts were determined by GC/MS/MS using exter-nal standard method. The linearity of the method was good between 5μg/L and 1000μg/L. In milk beverage, the mean recoveries at the three spiked levels of 10, 50, 200μg/kg were 80.9%-108.7%, the relative stan-dard deviation(RSD) were 0.2%-14.2%. In fruit drink, the mean recoveries at the three spiked levels of 10, 50, 200μg/kg were 81.4%-110.2%, the relative standard deviation (RSD) were 1.3%-13.0%. The detec-tion limits and quantitation limits were 1.5μg/kg-3.0μg/kg and 5.0μg/kg-10.0μg/kg respectively. The sim-plicity, sensitivity and good precision of the method made it be well suitable for determination of phthalate esters residues in drinks.%采用QuEChERS-气相色谱/三重四极杆质谱（GC/MS/MS）同时测定饮料中17种邻苯二甲酸酯类塑化剂。样品经正己烷提取，基质分散固相萃取净化，采用气相色谱-质谱/质谱法测定，外标法定量。17种邻苯二甲酸酯在各自的线性范围内（5μg/L～1000μg/L）线性关系良好，线性相关系数在0.99以上，添加10、50和200μg/kg 3个不同浓度水平，含乳饮料中17种邻苯二甲酸酯的平均回收率在80.9%～108.7%，相对标准偏差在0.2%～14.2%，果汁饮料中17种邻苯二甲酸酯的平均回收率在81.4%～110.2%，相对标准偏差在1.3%～13.0%，检出限和定量下限分别为1.5μg/kg～3.0μg/kg和5.0μg/kg～10.0μg/kg。该方法灵敏度高、重现性好、结果准确可靠，适合饮料中邻苯二甲酸酯类塑化剂的检测。
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