Synthesis of Click-Chelator via Cu(I)-Catalyzed Alkyne-Azide Cycloaddition

Yang Fu; Yan Liu; Xiaoping Fu; Li Zou; Hua Li; Ming Li; Prof. Dr. Xingguo Chen; Jingui Qin

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Synthesis of Click-Chelator via Cu(I)-Catalyzed Alkyne-Azide Cycloaddition

机译：铜（I）催化的炔-叠氮化物环加成反应合成点击螯合剂

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The click-ligands based on 1,2,3-triazole and pyridine unit has been synthesized via Cu(I)-catalyzed alkyne-azide cycloaddition from corresponding organic azides and terminal alkynes. The ligand structure was characterized by NMR, IR and elemental analysis as well as single crystal diffractions. The single crystal structure of the complexes from two different ligands coordinating to Cu(II) and Co(II) ions indicated that the N(2) atom in 1,2,3-triazole unit can act as an efficient donor to metals through the rational molecular design.

机译：基于1,2,3-三唑和吡啶单元的点击配体已通过Cu（I）催化的炔-叠氮化物环加成反应从相应的有机叠氮化物和末端炔烃合成。通过NMR，IR和元素分析以及单晶衍射来表征配体结构。来自两个不同配体与Cu（II）和Co（II）离子配位的配合物的单晶结构表明1,2,3-三唑单元中的N（2）原子可以通过合理的分子设计。

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来源
《Chinese Journal of Chemistry》 |2010年第11期|p.2226-2232|共7页
作者
Yang Fu; Yan Liu; Xiaoping Fu; Li Zou; Hua Li; Ming Li; Prof. Dr. Xingguo Chen; Jingui Qin;
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作者单位

Department of Chemistry and Hubei Key Laboratory on Organic and Polymeric Opto-Electronic Materials, Wuhan University, Wuhan, Hubei 430072, China;

College of Chemical Engineering, Wuhan Textile University, Wuhan, Hubei 430074, China;

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原文格式 PDF
正文语种 eng
中图分类
关键词
Click Chemistry; ligand design; N ligands; synthesis;

机译：点击化学;配体设计;N配体;合成;

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1. Synthesis of Click-Chelator via Cu(I)-Catalyzed Alkyne-Azide Cycloaddition [J] . Fu,Yang, Liu,Yan, Fu,Xiaoping, 中国化学（英文版） . 2010,第011期
2. Comparative analysis of Cu (I)-catalyzed alkyne-azide cycloaddition (CuAAC) and strain-promoted alkyne-azide cycloaddition (SPAAC) in O-GlcNAc proteomics [J] . Li Shanshan, Zhu He, Wang Jiajia, Electrophoresis: The Official Journal of the International Electrophoresis Society . 2016,第11期

机译：O-GlcNAc蛋白质组学中铜（I）催化炔叠氮化物环加成（CuAAC）和应变促进炔叠氮化物环加成（SPAAC）的比较分析
3. Cu(I)-catalyzed alkyne-azide "click' cycloaddition (CuAAC): a clean, efficient, and mild synthesis of new 1,4-disubstituted 1H-1,2,3-triazole-linked 2-amino-4,8-dihydropyrano[3,2-b]pyran-3-carbonitrile-crystal structure [J] . Aghbash Khadijeh Ojaghi, Pesyan Nader Noroozi, Sahin Ertan Research on Chemical Intermediates . 2019,第4期

机译：CU（i）-catalyzed alkyne-叠氮化物“点击”Cycloaddition（Cuaac）：新的1,4-二取代的1H-1,2,3-三唑连接的2-氨基-4,8的清洁，高效，轻度合成 -dihydropyrano [3,2-b]吡喃-3-碳腈 - 晶体结构
4. SYNTHESIS OF FUNCTIONALIZED ALIPHATIC POLYESTERS BY THE "CLICK" COPPER-CATALYZED ALKYNE-AZIDE CYCLOADDITION [C] . PHILIPPE LECOMTE, RAPHAEL RIVA, CHRISTINE JEROME NATO Advanced Study Institute on New Smart Materials via Metal Mediated Macromolecular Engineering: from Complex to Nano Structures . 2009

机译：通过“点击”铜催化的炔芳酮 - 叠氮化物环加成合成官能化脂族聚酯
5. Synthesis and characterization of cyclic polystyrene using copper-catalyzed alkyne-azide cycloaddition coupling - evaluation of physical properties and optimization of cyclization conditions. [D] . Elupula, Ravinder. 2016

机译：使用铜催化的炔-叠氮化物环加成偶联反应合成和表征环状聚苯乙烯-物理性质评估和环化条件优化。
6. Comparative analysis of Cu (I)-catalyzed alkyne-azide cycloaddition (CuAAC) and strain-promoted alkyne-azide cycloaddition (SPAAC) in O-GlcNAc proteomics [O] . Shanshan Li, He Zhu, Jiajia Wang, -1

机译：O-GlcNAc蛋白质组学中铜（I）催化炔叠氮化物环加成（CuAAC）和应变促进炔叠氮化物环加成（SPAAC）的比较分析
7. Comparative analysis of Cu (I)-catalyzed alkyne-azide cycloaddition (CuAAC) and strain-promoted alkyne-azide cycloaddition (SPAAC) inO-GlcNAc proteomics [O] . Shanshan Li, He Zhu, Jiajia Wang, 2016

机译：Cu（I）的对比分析 - 催化炔氧化物环加成（CuAAc）和菌株促进的炔氧化物环加成（Spaac）Ino-Glcnac蛋白质组学

Synthesis of Click-Chelator via Cu(I)-Catalyzed Alkyne-Azide Cycloaddition

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