• 主题
高级搜索  >
历史搜索 清空历史
首页> 外文期刊>Chromatographia >Determination of Iodate in Iodized Salt by Reversed-Phase High-Performance Liquid Chromatography with UV Detection
【24h】

Determination of Iodate in Iodized Salt by Reversed-Phase High-Performance Liquid Chromatography with UV Detection

机译：反相高效液相色谱-紫外检测法测定碘盐中的碘酸盐

获取原文
获取原文并翻译 | 示例
           
页面导航
  • 摘要
  • 著录项
  • 相似文献
  • 相关主题

摘要

A method for the determination of iodate was developed by reversed-phase high-performance liquid chromatography with UV detection. Iodate was converted to iodine, which was separated from the matrix using a reversed-phase Ultrasphere C18 column (250 × 4.6 mm, 5 μm) with methanol-1 mmol L−1 H3PO4 (20:80, v/v) as mobile phase at 1.00 mL min−1 and UV detection at 224 nm. The calibration graph was linear from 0.05 μg mL−1 to 5.00μg mL−1 for iodine with a correlation coefficient of 0.9994 (n=7). The detection limit was 0.01 μg mL−1. The method was successfully applied to the determination of iodate in iodized salt. The recovery was from 96% to 101% and the relative standard deviation was in the range of 1.5% to 2.9%.
机译：建立了反相高效液相色谱紫外检测法测定碘酸盐的方法。碘化物转化为碘，使用反相的Ultrasphere C18 色谱柱（250×4.6 mm，5μm）和甲醇-1 mmol L-1 H3 与碘分离。以1.00 mL min-1 作为流动相的PO4 （20:80，v / v）和224 nm处的UV检测。碘的校准曲线是线性的，从0.05μgmL-1 到5.00μgmL-1 ，相关系数为0.9994（n = 7）。检出限为0.01μgmL-1 。该方法已成功应用于碘盐中碘酸盐的测定。回收率为96％至101％，相对标准偏差为1.5％至2.9％。

著录项

  • 来源
    《Chromatographia》 |2004年第12期|721-723|共3页
  • 作者

    X. R. Xu; H. B. Li; J.-D. Gu; K. J. Paeng;

  • 作者单位

    Laboratory of Environmental Toxicology Department of Ecology Biodiversity The University of Hong Kong;

    Laboratory of Environmental Toxicology Department of Ecology Biodiversity The University of Hong KongDepartment of Chemistry Yonsei University;

    Laboratory of Environmental Toxicology Department of Ecology Biodiversity The University of Hong KongThe Swire Institute of Marine Science The University of Hong Kong;

    Department of Chemistry Yonsei University;

  • 收录信息
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    Column liquid chromatography; Lodate in iodized salt;

    机译：柱液相色谱;碘酸盐中的碘酸盐;

相似文献

  • 外文文献
  • 中文文献
  • 专利
获取原文

客服邮箱：kefu@zhangqiaokeyan.com

京公网安备：11010802029741号 ICP备案号：京ICP备15016152号-6 六维联合信息科技 (北京) 有限公司©版权所有

  • 客服微信

  • 服务号