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首页> 外文期刊>Clean technologies and environmental policy >Utilising high throughput technologies for the determination of the reaction network of the L-proline catalysed aldol reaction
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Utilising high throughput technologies for the determination of the reaction network of the L-proline catalysed aldol reaction

机译：利用高通量技术确定L-脯氨酸催化的羟醛反应的反应网络

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摘要

The objective of this work is to facilitate the determination of a reliable reaction network for the l-proline catalysed aldol reaction using high throughput technologies (HTT). The availability of reliable reaction network is fundamental to predictive kinetic modelling including scale up, replacing a batch process with a continuous one, optimisation. thermal safety, process simulation, etc. The extent to which HTT experiments may be used to provide the necessary quantitative understanding of both physical and chemical phenomena of the system studied is assessed through a four stage development programme. For this particular system it is shown that, in conjunction with appropriate experimental designs, meaningful data streams for mechanistic/kinetic studies can be generated. The experimental data allowed a reaction network for the L-proline catalysed aldol reaction to be proposed and verified through a kinetic modelling exercise.
机译：这项工作的目的是促进使用高通量技术（HTT）为l-脯氨酸催化的羟醛反应确定可靠的反应网络。可靠的反应网络的可用性是预测动力学建模的基础，包括扩大规模，以连续过程代替批量过程，进行优化。热安全性，过程仿真等。通过四个阶段的开发计划，可以评估HTT实验可用于提供所研究系统的物理和化学现象的必要定量理解的程度。对于该特定系统，表明与适当的实验设计相结合，可以生成有意义的数据流，用于机械/动力学研究。实验数据允许提出用于L-脯氨酸催化的醛醇缩合反应的反应网络，并通过动力学建模练习进行了验证。

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