An efficient method for synthesis of bis(indolyl)methane and di-bis(indolyl)methane derivatives in environmentally benign conditions using TBAHS

Sayed Hossein Siadatifard; Masumeh Abdoli-Senejani; Mohammad Ali Bodaghifard

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An efficient method for synthesis of bis(indolyl)methane and di-bis(indolyl)methane derivatives in environmentally benign conditions using TBAHS

机译：使用TBAHS在环境良性条件下合成双（吲哚基）甲烷和二双（吲哚基）甲烷衍生物的有效方法

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摘要

An efficient procedure for the synthesis of bisindolylmethanes from condensation of indole and aromatic aldehydes or ketones is described. The aromatic electrophilic substitution reactions of indole with aromatic aldehydes and ketones are achieved in the presence of tetrabutylammonium hydrogen sulfate as a mild and efficient solid acid catalyst. This methodology offers several advantages such as good yields, simple procedure, mild and environmentally benign conditions.

机译：描述了一种由吲哚与芳族醛或酮的缩合反应合成二吲哚基甲烷的有效方法。在作为温和有效的固体酸催化剂的硫酸四丁基铵存在下，吲哚与芳族醛和酮的芳族亲电取代反应得以实现。这种方法具有许多优点，例如产量高，操作简单，环境温和且环境友好。

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《Cogent Chemistry》 |2016年第1期|共7页
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Sayed Hossein Siadatifard; Masumeh Abdoli-Senejani; Mohammad Ali Bodaghifard;
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中图分类化学;
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1. PCl 5 as a mild and efficient catalyst for the synthesis of bis(indolyl)methanes and di-bis(indolyl)methanes | Hasaninejad | Bulletin of the Chemical Society of Ethiopia [J] . Alireza Hasaninejad, Abdolkarim Zare, Hashem Sharghi, Bulletin of the Chemical Society of Ethiopia . 2008,第3期

机译：PCl 5作为合成双（吲哚基）甲烷和二双（吲哚基）甲烷的温和高效催化剂| Hasaninejad |埃塞俄比亚化学会简报
2. Poly(N,N'-dichloro-N-ethyl-benzene-1, 3-disulfonamide) and N,N,N',N'-tetrachlorobenzene-1,3-disulfonamide as novel catalytic reagents for synthesis of bis-indolyl, tris-indolyl, di(bis-indolyl), tri(bis-indolyl) and tetra(bis-indolyl)methanes under solid-state, solvent and water conditions [J] . Hojat Veisi, Ramin Ghorbani-vaghei Journal of the Brazilian Chemical Society . 2010,第2期

机译：聚（N，N'-二氯-N-乙基苯-1,3-二磺酰胺）和N，N，N'，N'-四氯苯-1,3-二磺酰胺为合成双吲哚基的新型催化试剂，固态，溶剂和水条件下的三吲哚基甲烷，二（双吲哚基），三（双吲哚基）和四（双吲哚基）甲烷
3. Poly(N,N'-dichloro-N-ethyl-benzene-1, 3-disulfonamide) and N,N,N',N'-Tetrachlorobenzene-1,3-disulfonamide as Novel Catalytic Reagents for Synthesisof Bis-indolyl, Tris-indolyl, Di(bis-indolyl), Tri(bis-indolyl) and Tetra(bis-indolyl)Methanes under Solid-State, Solvent and Water Conditions [J] . Ramin Ghorbani-Vaghei, Hojat Veisi Journal of the Brazilian Chemical Society . 2010,第2期

机译：聚（N，N'-二氯-N-乙基苯-1,3-二磺酰胺）和N，N，N'，N'-四氯苯-1,3-二磺酰胺作为合成双吲哚基，Tris的新型催化试剂固态，溶剂和水条件下的-吲哚基，二（双-吲哚基），三（双-吲哚基）和四（双-吲哚基）甲烷
4. A mild, eco-friendly and efficient zeolite catalyzed synthesis of vibrindole A and bis(indolyl)methanes [C] . M. Karthik, M. Palanichamy, V. Murugesan International Symposium on Nanoporous Materials; 20050607-10; Niagara Falls(CA) . 2005

机译：温和，环保，高效的沸石催化合成纤颤素A和双（吲哚基）甲烷
5. Cytotoxicity of indole-ring substituted 1,1-bis (3'-indolyl)-1-(p-phenyl-t-butyl) methanes in colon cancer cells [D] . Newman, Kristin Laine. 2008

机译：吲哚环取代的1,1-双（3'-吲哚基）-1-（对苯基叔丁基）甲烷在结肠癌细胞中的细胞毒性
6. An Eco-Friendly Improved Protocol for the Synthesis of Bis(3-indolyl)methanes Using Poly(4-vinylpyridinium)hydrogen Sulfate as Efficient Heterogeneous and Recyclable Solid Acid Catalyst [O] . Janardhan Banothu, Rajitha Gali, Ravibabu Velpula, 2013

机译：聚（4-乙烯基吡啶鎓）硫酸氢盐为高效多相和可循环使用的固体酸催化剂用于合成双（3-吲哚基）甲烷的生态友好型改进方案
7. An efficient method for synthesis of bis(indolyl)methane and di-bis(indolyl)methane derivatives in environmentally benign conditions using TBAHS [O] . Seyed Hossein Siyadatifard, Masumeh Abdoli-Senejani, Mohammad Ali Bodaghifard 2016

机译：使用TBaHs在环境友好条件下合成双（吲哚基）甲烷和二 - 双（吲哚基）甲烷衍生物的有效方法

An efficient method for synthesis of bis(indolyl)methane and di-bis(indolyl)methane derivatives in environmentally benign conditions using TBAHS

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