One-pot synthesis of 2 a?? phenylimidazo [4, 5-f] [1, 10] phenanthroline derivatives under solvent free conditions by using iodine

Syed shahed ali

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One-pot synthesis of 2 a?? phenylimidazo [4, 5-f] [1, 10] phenanthroline derivatives under solvent free conditions by using iodine

机译：一锅合成2 a ??碘法在无溶剂条件下生成苯基咪唑并[4，5-f] [1，10]菲咯啉衍生物

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2 - Phenylimidazo[4, 5-f][1, 10]phenanthrolines could be obtained in excellent yields by the onepot three-component condensation of 1, 10 phenanthroline-5,6-dione, aldehyde and ammonium acetate in the presence of catalytic amount of the inexpensive, readily available iodine under solvent-free condition. The mixture was ground together in a mortar with a pestle at room temperature for short reaction time and easy operation under solvent free condition.

机译：在催化作用下，通过1,10菲咯啉-5,6-二酮，醛和乙酸铵的一锅式三组分缩合反应，可以得到2-苯基咪唑并[4,5-f] [1,10]菲咯啉。在无溶剂条件下的少量廉价，易于获得的碘。将该混合物在室温下用研钵在研钵中一起研磨，以缩短反应时间，并易于在无溶剂条件下操作。

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《Archives of Applied Science Research》 |2010年第5期|共页
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Syed shahed ali;
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1. Potassium ferro-cyanide trihydrate complex catalyzed one-pot synthesis of 2-phenylimidazo 4,5-f 1,10 phenanthroline [J] . Syed Shahed Ali 中国化学快报（英文版） . 2011,第007期

机译：三水合亚铁氰化钾催化一锅合成2-苯基咪唑并4,5-f 1,10菲咯啉
2. Potassium ferro-cyanide trihydrate complex catalyzed one-pot synthesis of 2-phenylimidazo 4,5-f 1,10 phenanthroline [J] . Syed Shahed Ali 中国化学快报：英文版 . 2011,第007期

机译：三水合亚铁氰化钾催化一锅合成2-苯基咪唑并4,5-f 1,10菲咯啉
3. Ruthenium(II) Complexes with 2-Phenylimidazo[4,5-f][1,10]phenanthroline Derivatives that Strongly Combat Cisplatin-Resistant Tumor Cells [J] . Leli Zeng, Yu Chen, Jiangping Liu, Scientific reports. . 2016,第1期

机译：钌（II）与2-苯基咪唑并[4,5-f] [1,10]菲咯啉衍生物的络合物可强烈抵抗顺铂耐药的肿瘤细胞
4. Highly efficient, one-pot, solvent-free synthesis of highly substituted imidazoles using molecular iodine as catalyst [C] . Yi-Ming Ren, Chun Cai International Conference on Chemical, Material and Metallurgical Engineering . 2012

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One-pot synthesis of 2 a?? phenylimidazo [4, 5-f] [1, 10] phenanthroline derivatives under solvent free conditions by using iodine

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