Improved Synthesis of 5-Aryl-2-thioxoimidazolidin-4-ones from Arylglyoxals Hydrates

Vasiliy Georgievich Shtamburg; Andrey Alexandrovich Anishchenko; Victor Vasilievich Shtamburg; Alexander Vladimirovich Mazepa; Svetlana Vladimirovna Kravchenko; Evgeniy Alexandrovich Klots

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Improved Synthesis of 5-Aryl-2-thioxoimidazolidin-4-ones from Arylglyoxals Hydrates

机译：由芳基乙二醛水合物改进的5-芳基-2-硫代氧杂咪唑啉-4-酮的合成

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摘要

New kind of 5-aryl-2-thioxoimidazolidin-4-ones synthesis by condensation of arylglyoxal hydrates with thiourea in acetic acid solution at room temperatures has been developed.

机译：通过在室温下乙酸溶液中芳基乙二醛水合物与硫脲的缩合反应，开发了一种新型的5-芳基-2-硫代氧杂咪唑啉丁-4-酮合成方法。

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《European Chemical Bulletin》 |2017年第5期|共4页
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Vasiliy Georgievich Shtamburg; Andrey Alexandrovich Anishchenko; Victor Vasilievich Shtamburg; Alexander Vladimirovich Mazepa; Svetlana Vladimirovna Kravchenko; Evgeniy Alexandrovich Klots;
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1. Regioselective N-1 and C-2 diacylation of 3-substituted indoles with arylglyoxal hydrates for the synthesis of indolyl diketones [J] . Dalong Pan, Jinpeng Chu, Xianrui Gao, Organic & biomolecular chemistry . 2018,第38期

机译：3-取代的吲哚与芳基乙二醛水合物的区域选择性N-1和C-2二酰化，用于合成吲哚基二酮
2. Copper-catalyzed synthesis of indolyl diketones via C-H oxidation/diacylation of indoles with arylglyoxal hydrates [J] . Cuiping Wang, Zhiqiang Zhang, Kui Liu, Organic & biomolecular chemistry . 2017,第29期

机译：通过芳基乙二醛水合物的吲哚的C-H氧化/二酰化反应，铜催化合成吲哚基二酮
3. Single-stage synthesis of 3-hydroxy- and 3-alkoxy-5-arylimidazolidine-2,4-diones by reaction of arylglyoxal hydrates with N-hydroxy- and N-alkoxyureas [J] . Shtamburg Vasiliy G., Shtamburg Viktor V., Anishchenko Andrey A., Chemistry of heterocyclic compounds . 2015,第6期

机译：通过芳基乙二醛水合物与N-羟基和N-烷氧基脲反应，单阶段合成3-羟基和3-烷氧基-5-芳基咪唑烷-2,4-二酮
4. Influence of the water temperature in the working area on the synthesis of gas hydrate by the method of boiling-condensation of the hydrate-forming gas in the volume of water [C] . Anton V. Meleshkin, Vitaly V. Glezer, Nikita V. Marasanov, Thermophysical Basis of Energy Technologies (conference) . 2021

机译：水温在水合物中水合物合成气体水合物的影响水合物在水体积体积中的沸腾凝结方法
5. A study of the xenon effect in type-II clathrate hydrate synthesis; Commencing with hydrogen, argon and xenon uptake into a propane clathrate hydrate. [D] . Abbondondola, Joanne Angela. 2008

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6. Organocatalytic Asymmetric Aldol Reaction of Arylglyoxals and Hydroxyacetone: Enantioselective Synthesis of 23-Dihydroxy-14-diones [O] . Yu-Hao Zhou, Yu-Zu Zhang, Zhu-Lian Wu, 2020

机译：芳基乙二醛与羟丙酮的有机催化不对称羟醛反应：23-二羟基-14-二酮的对映选择性合成
7. Efficient synthesis of novel 1-hydroxy-2,4,5-trisubstituted imidazole derivatives via a one-pot, four-component reaction between hydroxylamine, benzonitriles, arylglyoxals and 1,3-dicarbonyl compounds [O] . Farzaneh Alizadeh-Bami, Mina Salehzadeh, Hossein Mehrabi, 2019

机译：通过单罐，羟胺，苯腈，芳基乙醛和1,3-二羰基化合物之间的一种罐，四组分反应有效合成新的1-羟基-2,4,5-三取代的咪唑衍生物
8. Methane Hydrate Synthesis in the DOE/METC Gas Hydrates Laboratory: Technical Note [R] . Dominic, K. 1986

机译：DOE / mETC天然气水合物实验室中的甲烷水合物合成：技术说明

Improved Synthesis of 5-Aryl-2-thioxoimidazolidin-4-ones from Arylglyoxals Hydrates

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