Synthesis and characterization of new 1,2-diazepine derivative

Majal Sapnakumari; Badiadka Narayana; Seranthimata Samshuddin; Balladka Kunhanna Sarojini

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Synthesis and characterization of new 1,2-diazepine derivative

机译：新的1,2-二氮杂pine衍生物的合成与表征

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The reaction of (1Z)-1-[(2E)-3-(4-bromophenyl)-1-(4-fluorophenyl)prop-2-en-1-ylidene]-2-(2,4-dinitrophenyl) hydrazine (2) with ethyl chloroacetate in the presence of base affords a new 1,2-diazepine derivative, 5-(4- bromophenyl)-1-(2,4-dinitrophenyl)-3-(4-fluorophenyl)-1H-1,2-diazepin-6-ol (3). The intermediate 2 in turn prepared from 4-bromo-4'-fluorochalcone (1). The structure of the newly synthesized compound is characterized by IR, NMR and mass spectral data.

机译：（1Z）-1-[（2E）-3-（4-溴苯基）-1-（4-氟苯基）丙-2-烯-1-亚烷基] -2-（2,4-二硝基苯基）肼的反应（2）在碱的存在下用氯乙酸乙酯得到新的1,2-二氮杂derivative衍生物5-（4-溴苯基）-1-（2,4-二硝基苯基）-3-（4-氟苯基）-1H-1 ，2-二氮杂-1-醇（3）。中间体2又由4-溴-4'-氟查耳酮（1）制备。新合成的化合物的结构通过IR，NMR和质谱数据表征。

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《Der Pharma Chemica: journal for medicinal chemistry, pharmaceutical chemistry and computational chemistry》 |2012年第6期|共4页
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Majal Sapnakumari; Badiadka Narayana; Seranthimata Samshuddin; Balladka Kunhanna Sarojini;
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机译：有机锂路由到1,2-二取代乙烯衍生物。试图合成1,2-二硫代乙烯。

Synthesis and characterization of new 1,2-diazepine derivative

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