Crystal structure of catena-poly[[(N,N-diethyl-3-mesitylsulfonyl-1H-1,2,4-triazole-1-carboxamide-κN1)silver(I)]-μ-nitrato-κ3O,O′:O]

Park H.; Kwon E.; Yoon I.; Kim J.

首页> 外文期刊>Acta Crystallographica Section E: Crystallographic Communications >Crystal structure of catena-poly[[(N,N-diethyl-3-mesitylsulfonyl-1H-1,2,4-triazole-1-carboxamide-κN1)silver(I)]-μ-nitrato-κ3O,O′:O]

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Crystal structure of catena-poly[[(N,N-diethyl-3-mesitylsulfonyl-1H-1,2,4-triazole-1-carboxamide-κN1)silver(I)]-μ-nitrato-κ3O,O′:O]

机译：链状聚[[（（N，N-二乙基-3-甲磺酰基磺酰基-1H-1,2,4-三唑-1-羧酰胺-κN1）]银（I）]-μ-硝基-κ3O，O'的晶体结构： O]

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摘要

The reaction of silver nitrate and cafenstrole (N,N-diethyl-3-mesitylsulfonyl-1H-1,2,4-triazole-1-carboxamide), a triazole herbicide, leads to the title coordination polymer, [Ag(NO3)(C16H22N4O3S)]n, whose asymmetric unit comprises one cafenstrole ligand molecule, one AgI atom and one nitrate ion. The AgI atom, with a distorted trigonal–pyramidal environment, is coordinated by one nitrogen atom of a triazole ring, two oxygen atoms of a nitrate ion and one oxygen atom of a neighboring nitrate ion. The coordination bonds between silver and oxygen atoms give rise to a one-dimensional (1D) coordination polymer structure along [001]. The dihedral angle between the planes of the triazole and benzene rings is 87.13 (11)°. In the crystal, the coordination polymer is stabilized by C—H⋯O hydrogen bonds and C—H⋯π interactions, resulting in a three-dimensional architecture.

机译：三唑类除草剂硝酸银与咖啡酚（N，N-二乙基-3-甲磺酰基磺酰基-1H-1,2,4-三唑-1-羧酰胺）的反应生成标题配位聚合物[Ag（NO3） C 16 H 22 N 4 O 3 S）] n，其不对称单元包含一个咖啡甾醇配体分子，一个AgI原子和一个硝酸根离子。 AgI原子具有扭曲的三角锥锥体环境，由三唑环的一个氮原子，硝酸根离子的两个氧原子和相邻的硝酸根离子的一个氧原子配位。银和氧原子之间的配位键沿[001]形成一维（1D）配位聚合物结构。三唑和苯环平面之间的二面角为87.13（11）°。在晶体中，配位聚合物通过CHHO氢键和CHHπ相互作用而稳定，从而形成三维结构。

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《Acta Crystallographica Section E: Crystallographic Communications》 |2016年第11期|共4页
作者
Park H.; Kwon E.; Yoon I.; Kim J.;
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中图分类晶体学;
关键词
CRYSTAL STRUCTURECAFENSTROLECOORDINATION POLYMERSILVERTRIAZOLEHERBICIDE;

机译：结晶结构阳离子弹性配位聚合物;

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Crystal structure of catena-poly[[(N,N-diethyl-3-mesitylsulfonyl-1H-1,2,4-triazole-1-carboxamide-κN1)silver(I)]-μ-nitrato-κ3O,O′:O]

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