PhI(OAc)2 oxidative C5 halogenation of quinolines using copper halides under mild conditions

Xing-Xing Liu; Zhao-Yang Wu; Xin-Liang Luo; Yong-Qin He; Xiao-Qiang Zhou; Yu-Xing Fan; Guo-Sheng Huang

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PhI(OAc)2 oxidative C5 halogenation of quinolines using copper halides under mild conditions

机译：PHI（OAC）2在温和条件下使用铜卤化氧化喹啉的氧化C5卤化

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A concise and efficient protocol for PhI(OAc) _(2) oxidation halogenation of quinoline at the C5 position was developed, affording the desired remote C–H activation products in moderate to excellent yields. This reaction proceeds with copper halides as the halogenating reagent to afford the halogenated quinolines and features excellent substrate tolerance, providing a facile pathway for the C5 halogenation of quinoline.

机译：开发了一种简明而有效的PHI（OAC）_（2）氧化喹啉在C5位置的氧化卤化，得到所需的远程C-H活化产物，其中等至优异的产率。该反应与卤化铜作为卤化试剂进行，得到卤代喹啉，具有优异的基底耐受性，为喹啉的C5卤化提供容易途径。

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《RSC Advances》 |2016年第75期|共4页
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Xing-Xing Liu; Zhao-Yang Wu; Xin-Liang Luo; Yong-Qin He; Xiao-Qiang Zhou; Yu-Xing Fan; Guo-Sheng Huang;
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1. PhI(OAc)(2) oxidative C5 halogenation of quinolines using copper halides under mild conditions [J] . Liu Xing-Xing, Wu Zhao-Yang, Luo Xin-Liang, RSC Advances . 2016,第75期

机译：PHI（OAC）（2）在温和条件下使用铜卤化氧化喹啉的氧化C5卤化
2. Copper(Ⅱ)-catalyzed C5 and C7 halogenation of quinolines using sodium halides under mild conditions [J] . Jun Xu, Xiaolei Zhu, Guobin Zhou, Organic & biomolecular chemistry . 2016,第11期

机译：铜（Ⅱ）在温和条件下用卤化钠催化喹啉的C5和C7卤化
3. The regioselective C5 halogenation of quinolines using sodium halides under transition metal-free conditions [J] . Jiao Jun-Ying, Mao Yuan Jun, Feng An-Wei, Tetrahedron . 2017,第11期

机译：在过渡金属条件下使用卤化钠的喹啉的区域选择性C5卤化
4. Oxidation of Organic Compounds by Phenyliodine Diacetate (PhI(OAc)2) as an Eco-Friendly Reagent in the Presence of Manganese Porphyrins as Biologically Relevant Catalysts [C] . Gholamreza Karimipour 2011 2nd International Conference on Chemistry and Chemical Engineering . 2011

机译：锰卟啉作为生物相关催化剂时，苯乙酸碘二乙酸酯（PhI（OAc）2）作为一种生态友好的试剂氧化有机化合物
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6. Regioselective chlorination and bromination of unprotected anilines under mild conditions using copper halides in ionic liquids [O] . Han Wang, Kun Wen, Nurbiya Nurahmat, 2012

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PhI(OAc)2 oxidative C5 halogenation of quinolines using copper halides under mild conditions

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