PhI(OAc)(2) oxidative C5 halogenation of quinolines using copper halides under mild conditions

Liu Xing-Xing; Wu Zhao-Yang; Luo Xin-Liang; He Yong-Qin; Zhou Xiao-Qiang; Fan Yu-Xing; Huang Guo-Sheng

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PhI(OAc)(2) oxidative C5 halogenation of quinolines using copper halides under mild conditions

机译：PHI（OAC）（2）在温和条件下使用铜卤化氧化喹啉的氧化C5卤化

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摘要

A concise and efficient protocol for PhI(OAc)(2) oxidation halogenation of quinoline at the C5 position was developed, affording the desired remote C-H activation products in moderate to excellent yields. This reaction proceeds with copper halides as the halogenating reagent to afford the halogenated quinolines and features excellent substrate tolerance, providing a facile pathway for the C5 halogenation of quinoline.

机译：开发了一种简明且有效的Phi（OAC）（2）氧化卤化在C5位置的氧化卤化，得到所需的远程C-H活化产物，其中等至优异的产率。该反应与卤化铜作为卤化试剂进行，得到卤代喹啉，具有优异的基底耐受性，为喹啉的C5卤化提供容易途径。

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来源
《RSC Advances》 |2016年第75期|共4页
作者
Liu Xing-Xing; Wu Zhao-Yang; Luo Xin-Liang; He Yong-Qin; Zhou Xiao-Qiang; Fan Yu-Xing; Huang Guo-Sheng;
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Lanzhou Univ Dept Chem State Key Lab Appl Organ Chem Key Lab Nonferrous Met Chem &

Resources Utilizat Lanzhou 730000 Peoples R China;

Lanzhou Univ Dept Chem State Key Lab Appl Organ Chem Key Lab Nonferrous Met Chem &

Resources Utilizat Lanzhou 730000 Peoples R China;

Lanzhou Univ Dept Chem State Key Lab Appl Organ Chem Key Lab Nonferrous Met Chem &

Resources Utilizat Lanzhou 730000 Peoples R China;

Lanzhou Univ Dept Chem State Key Lab Appl Organ Chem Key Lab Nonferrous Met Chem &

Resources Utilizat Lanzhou 730000 Peoples R China;

Lanzhou Univ Dept Chem State Key Lab Appl Organ Chem Key Lab Nonferrous Met Chem &

Resources Utilizat Lanzhou 730000 Peoples R China;

Lanzhou Univ Dept Chem State Key Lab Appl Organ Chem Key Lab Nonferrous Met Chem &

Resources Utilizat Lanzhou 730000 Peoples R China;

Lanzhou Univ Dept Chem State Key Lab Appl Organ Chem Key Lab Nonferrous Met Chem &

Resources Utilizat Lanzhou 730000 Peoples R China;

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正文语种 eng
中图分类化学;
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1. PhI(OAc)(2) oxidative C5 halogenation of quinolines using copper halides under mild conditions [J] . Liu Xing-Xing, Wu Zhao-Yang, Luo Xin-Liang, RSC Advances . 2016,第75期

机译：PHI（OAC）（2）在温和条件下使用铜卤化氧化喹啉的氧化C5卤化
2. Copper(Ⅱ)-catalyzed C5 and C7 halogenation of quinolines using sodium halides under mild conditions [J] . Jun Xu, Xiaolei Zhu, Guobin Zhou, Organic & biomolecular chemistry . 2016,第11期

机译：铜（Ⅱ）在温和条件下用卤化钠催化喹啉的C5和C7卤化
3. The regioselective C5 halogenation of quinolines using sodium halides under transition metal-free conditions [J] . Jiao Jun-Ying, Mao Yuan Jun, Feng An-Wei, Tetrahedron . 2017,第11期

机译：在过渡金属条件下使用卤化钠的喹啉的区域选择性C5卤化
4. Oxidation of Organic Compounds by Phenyliodine Diacetate (PhI(OAc)2) as an Eco-Friendly Reagent in the Presence of Manganese Porphyrins as Biologically Relevant Catalysts [C] . Gholamreza Karimipour 2011 2nd International Conference on Chemistry and Chemical Engineering . 2011

机译：锰卟啉作为生物相关催化剂时，苯乙酸碘二乙酸酯（PhI（OAc）2）作为一种生态友好的试剂氧化有机化合物
5. Homogeneous Catalytic Oxidation of Ammonia Under Mild Conditions [D] . Habib Zadeh, Faezeh. 2019

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6. Regioselective chlorination and bromination of unprotected anilines under mild conditions using copper halides in ionic liquids [O] . Han Wang, Kun Wen, Nurbiya Nurahmat, 2012

机译：在离子液体中使用卤化铜在温和条件下对未保护的苯胺进行区域选择性氯化和溴化
7. HALOGENATION OF OLEFINS INVOLVING EPOXIDES AND HALIDES OF AMIDES OF SULFONIC ACIDS-A PATHWAY TO THE SYNTHESIS OF HALOIDS HALOGENATION OF OLEFINS INVOLVING EPOXIDES AND HALIDES OF AMIDES OF SULFONIC ACIDS-A PATHWAY TO THE SYNTHESIS OF HALOIDS [O] . Hasan Khoca Khojaev 2017

机译：烯烃的卤化烯烃和磺酸酰胺的卤化物 - 一种途径偏离烯烃卤素的途径，涉及磺酸环氧化物的环氧化和卤化物 - 一种途径的途径

PhI(OAc)(2) oxidative C5 halogenation of quinolines using copper halides under mild conditions

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