Copper and triphenylphosphine-promoted sulfenylation of quinones with arylsulfonyl chlorides

Xiaoli Yu; Qiujin Wu; Huida Wan; Zhaojun Xu; Xingle Xu; Dawei Wang

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Copper and triphenylphosphine-promoted sulfenylation of quinones with arylsulfonyl chlorides

机译：用芳基磺酰氯促进醌醌的铜膦酰基化醌

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The efficient copper and triphenylphosphine-promoted sulfenylation of quinones with arylsulfonyl chlorides has been developed under mild conditions with moderate to good yields. Significantly, this provides an alternative method to synthesise arylthioquinone derivatives. This is the first time that arylthioquinones with arylsulfonyl chlorides as starting material have been prepared, which avoids the use of the awful smelling thioalcohols and thiophenols.

机译：在温和条件下，在温和的条件下开发了高效铜和三苯基膦溶解的醌醌与芳基氯化物的亚砜化。显着地，这提供了合成芳基喹啉衍生物的替代方法。这是第一次制备与芳基磺酰氯作为起始原料的芳基醌，这避免了使用可怕的嗅觉硫代醇和噻吩酚。

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《RSC Advances》 |2016年第67期|共4页
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Xiaoli Yu; Qiujin Wu; Huida Wan; Zhaojun Xu; Xingle Xu; Dawei Wang;
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1. Copper and triphenylphosphine-promoted sulfenylation of quinones with arylsulfonyl chlorides [J] . Yu Xiaoli, Wu Qiujin, Wan Huida, RSC Advances . 2016,第67期

机译：铜和三苯基膦促进的芳基磺酰氯对醌的亚磺酰基化
2. Synthesis of arylsulfonyl-quinones and arylsulfonyl-1,4-diols as FabH inhibitors: Pd-catalyzed direct C-sulfone formation by C-S coupling of quinones with arylsulfonyl chloride [J] . Bingyang Ge, Dawei Wang, Weifu Dong Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2014,第40期

机译：FabH抑制剂的芳基磺酰基-醌和芳基磺酰基-1,4-二醇的合成：醌与芳基磺酰氯的C-S偶联，钯催化直接C-砜的形成
3. Synthesis of arylsulfonyl-quinones and arylsulfonyl-1,4-diols as FabH inhibitors: Pd-catalyzed direct C-sulfone formation by C-S coupling of quinones with arylsulfonyl chloride [J] . Bingyang Ge, Dawei Wang, Weifu Dong Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2014,第40期

机译：FabH抑制剂的芳基磺酰基-醌和芳基磺酰基-1,4-二醇的合成：醌与芳基磺酰氯的C-S偶联，钯催化直接C-砜的形成
4. Copper-Catalyzed Sulfenylation of Alkenes Using Thiols [C] . Nobukazu Taniguchi 日本化学会春季年会講演予稿集 . 2018

机译：使用硫醇铜催化烯烃的磺酰化
5. Kinetics and Transport Phenomena in the Chemical Decomposition of Copper Oxychloride in the Thermochemical Copper Chloride Cycle. [D] . Marin, Gabriel D. 2012

机译：氯化铜热化学循环中三氯氧化铜化学分解的动力学和输运现象。
6. General scheme of the phosphotriester condensation in the oligodeoxyribonucleotide synthesis with arylsulfonyl chlorides and arylsulfonyl azolides. [O] . V F Zarytova, D G Knorre 1984

机译：寡脱氧核糖核苷酸与芳基磺酰氯和芳基磺酰偶氮化物合成中的磷酸三酯缩合的一般流程。
7. A copper-induced quinone degradation pathway provides protection against combined copper/quinone stress in Lactococcus lactis IL1403. [O] . Mancini Stefano, Abicht Helge, Gonskikh Yulia, 2015

机译：铜诱导的醌降解途径为乳酸乳球菌IL1403中的铜/醌组合应力提供了保护。
8. The Interaction of Hydrazine with Copper(II) Chloride in Acidic Solutions. The Formation, Spectral and Magnetic Properties, and Structures of Copper(II), Copper(I), and Mixed Valence Species. [R] . Brown, D. B., Donner, J. A., Hall, J. W., 1979

机译：肼与氯化铜（II）在酸性溶液中的相互作用。铜（II），铜（I）和混合价物种的形成，光谱和磁性以及结构。

Copper and triphenylphosphine-promoted sulfenylation of quinones with arylsulfonyl chlorides

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