Rapid Z-plate seed regeneration of large size KDP crystal from solution

Guohui Li

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Rapid Z-plate seed regeneration of large size KDP crystal from solution

机译：从溶液中快速扩增大尺寸KDP晶体的Z板种子

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摘要

Regeneration process of a 330 × 330 × 20 mm~3 Z-plate seed is carried out in a 1.5 metric tonnage volume crystallizer that placed in a water bath of temperature fluctuation less than ±0.02 ℃ within 10 days. The surface of the whole crystal was restored by the formation of a box-like structure filled with growth solution, and then the transparent layer of perfect tetragonal KDP crystal without inclusions, crack and milky regions just like those produced by traditional slow cooling technique can be grown from solution. After the regeneration, the height of KDP crystal is merely 0.5 times the side of plate seed. We found it that the optical transmission and laser damage threshold of the KDP crystals we grown are not significantly different from those of KDP crystals grown by traditional method.

机译：在放置于温度波动小于±0.02℃的水浴中的1.5公吨体积的结晶器中，在10天内对330×330×20 mm〜3 Z板种子进行再生处理。通过形成填充有生长溶液的盒状结构来恢复整个晶体的表面，然后可以像传统的缓慢冷却技术所产生的那样，形成完美的四方KDP晶体透明层，而没有夹杂物，裂纹和乳状区域。从解决方案中成长。再生后，KDP晶体的高度仅为板晶侧面的0.5倍。我们发现，我们生长的KDP晶体的光学透射率和激光损伤阈值与传统方法生长的KDP晶体没有显着差异。

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来源
《Journal of Crystal Growth》 |2008年第1期|p.36-39|共4页
作者
Guohui Li;
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作者单位

Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou 350002, People's Republic of China;

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收录信息美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
原文格式 PDF
正文语种 eng
中图分类晶体学;
关键词
B1. KDP crystal; A1. rapid regeneration; A1. large size Z-plate seed;

机译：B1。 KDP晶体;A1。快速再生;A1。大号Z板种子;

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1. Quality of KDP Crystals Grown on Point Seeds by a Novel Rapid Growth Method [J] . E. L. Kim, V. I. Katsman, V. V. Vorontsov, Inorganic materials . 2008,第8期

机译：一种新型快速生长方法在点种子上生长的KDP晶体的质量
2. Hydrodynamics of Solution for the Rapid Growth of KDP Crystals [J] . Verezub N. A., Voloshin A. E., Manomenova V. L., Crystallography reports . 2018,第2期

机译：KDP晶体快速生长的溶液流体动力学
3. Improvement of growth rate and optical performances of rapidly grown KDP crystal by adding cyclohexane diamine tetraacetic acid in growth solution [J] . Shengjun Zhu, Shenglai Wang, Jianxu Ding, Journal of Crystal Growth . 2014,第feba15期

机译：通过在生长溶液中加入环己烷二胺四乙酸提高KDP晶体的生长速度和光学性能
4. Structural quality of the interface seed crystal in rapidly grown KDP crystals for high-power lasers [C] . V.I. Salo, Institute for Single Crystals, Kharkov, Symposium on optical materials for high-power lasers . 1999

机译：高功率激光器快速生长的KDP晶体中界面晶种的结构质量
5. OPTICAL PROPERTIES OF KDP TYPE CRYSTALS IN THE LOW-WAVENUMBER REGION [D] . Kawamura, Tetsuo -1

机译：低波数区域中KDP型晶体的光学性质
6. KDP Aqueous Solution-in-Oil Microemulsion for Ultra-Precision Chemical-Mechanical Polishing of KDP Crystal [O] . Hui Dong, Lili Wang, Wei Gao, 2017

机译：KDP油包水型微乳液用于KDP晶体的超精密化学机械抛光
7. Rapid growth of a long-seed KDP crystal [O] . Duanyang Chen, Bin Wang, Hu Wang, 2020

机译：长种子KDP晶体的快速生长
8. Rapid Growth of Very Large KDP and KD*P Crystals in Support of the National Ignition Facility. [R] . Hawley-Fedder, R., Robey, H., Biesiada, T., 2000

机译：支持国家点火装置的超大KDp和KD * p晶体的快速增长。

Rapid Z-plate seed regeneration of large size KDP crystal from solution

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