Ionothermal Synthesis Of Microporous Aluminum And Gallium Phosphates

Lijun Han; Yibo Wang; Suojiang Zhang; Xingmei Lu

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Ionothermal Synthesis Of Microporous Aluminum And Gallium Phosphates

机译：电热合成微孔铝和镓磷酸盐

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摘要

Four aluminum and gallium phosphates including AIPO_4-quartz (1), GaPO_4-quartz (2), AIPO_4-LTA (3) and GaPO_4-LTA (4) were ionothermally synthesized using [Emim]Bras structure-directing agent (SDA) and solvent. The samples were characterized by scanning electron micrographs (SEM), X-ray single crystal diffraction and X-ray powder diffraction (XRD). Effects of synthesis conditions, such as P_2O_5/ Al_2O_3 and HF/Al_2O_3 ratios, as well as P_2O_5/Ga_2O_3 ratio and reaction temperature on the crystallization of aluminum and gallium phosphates were investigated, respectively. It was indicated that the P_2O_5/Al_2O_3 ratio or P_2O_5/Ga_2O_3 ratio played the dominant role in the phase transformation of aluminum phosphates or gallium phosphates.

机译：使用[Emim] Bras结构导向剂（SDA）和溶剂离子热合成了四种磷酸铝和镓磷酸盐，包括AIPO_4-石英（1），GaPO_4-石英（2），AIPO_4-LTA（3）和GaPO_4-LTA（4）。。通过扫描电子显微镜（SEM），X射线单晶衍射和X射线粉末衍射（XRD）对样品进行表征。分别研究了P_2O_5 / Al_2O_3和HF / Al_2O_3比，P_2O_5 / Ga_2O_3比，反应温度等合成条件对磷酸铝和磷酸镓结晶的影响。结果表明，P_2O_5 / Al_2O_3比或P_2O_5 / Ga_2O_3比在磷酸铝或磷酸镓的相变中起主要作用。

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来源
《Journal of Crystal Growth》 |2008年第1期|p.167-171|共5页
作者
Lijun Han; Yibo Wang; Suojiang Zhang; Xingmei Lu;
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作者单位

Key Laboratory of Green process and Engineering, Institute of Process Engineering, Chinese Academy of Sciences, Beijing, 100190, PR China;

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收录信息美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
原文格式 PDF
正文语种 eng
中图分类晶体学;
关键词
a1. single crystal growth; a1. characterization; a2. growth from melt; b1. phosphates; b1. gallium compounds;

机译：a1。单晶生长;a1。表征;a2。从熔体中生长;b1。磷酸盐;b1。镓化合物;

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1. The role of added water in the ionothermal synthesis of microporous aluminium phosphates [J] . David S. Wragg, Alexandra M.Z. Slawin, Russell E. Morris Solid state sciences . 2009,第2期

机译：加水在微孔磷酸铝离子热合成中的作用
2. The ionothermal synthesis and properties of new gallium phosphates substituted by Co and Fe [J] . Fu Xiao-Fang, Lei Lian-Cai, Yang Jun-Qing, Polyhedron: The International Journal for Inorganic and Organometallic Chemistry . 2018,第期

机译：由CO和Fe取代的新镓磷酸盐的离子炎性合成及性质
3. Ionothermal synthesis, characterization of a new layered gallium phosphate with an unusual heptamer SBU [J] . Gao Fan, Huang Liangliang, Ma Yike, Journal of Solid State Chemistry . 2017,第期

机译：离子液合成，具有不寻常的七肽SBU的新分层磷酸盐的表征
4. Ionothermal Synthesis and Electrochemical Characterization of Nanostructured Lithium Manganese Phosphates [C] . P. Barpanda, N. Recham, K. Djellab, Symposium on intercalation compounds for lithium batteries . 2010

机译：纳米结构锂锰磷酸盐的离子炎性合成与电化学表征
5. Fundamental research of the solvent role in the ionothermal synthesis of microporous materials. [D] . Sun, Xin. 2012

机译：溶剂在微孔材料电热合成中的作用基础研究。
6. Characterization of Gallium Indium Phosphide and Progress of Aluminum Gallium Indium Phosphide System Quantum-Well Laser Diode [O] . Hiroki Hamada 2017

机译：镓铟磷化物的表征及铝镓磷化物体系量子阱激光二极管的研究进展
7. Ionothermal synthesis and electrochemical characterization of nanostructured lithium manganese phosphates [O] . Barpanda P., Recham N., Djellab K., 2010

机译：纳米结构磷酸锂锰的电热合成和电化学表征
8. The Attempted Syntheses of Low Oxidation State, Organometallic Derivatives of Aluminum, Gallium and Indium, a New Synthesis of Al(CH2SiMe3)3 [R] . Beachley, O. T., Tessier-Youngs, C., Simmons, R. G., 1981

机译：低氧化态的尝试合成，铝，镓和铟的有机金属衍生物，al（CH2sime3）3的新合成

Ionothermal Synthesis Of Microporous Aluminum And Gallium Phosphates

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