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首页> 外文期刊>Journal of the Institute of Brewing >HS-SPME/GC-MS and chemometrics for volatile composition of Chinese traditional aromatic vinegar in the Zhenjiang region
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HS-SPME/GC-MS and chemometrics for volatile composition of Chinese traditional aromatic vinegar in the Zhenjiang region

机译：镇江地区中国传统香醋挥发性成分的HS-SPME / GC-MS和化学计量学

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摘要

The main purpose of this study was to determine the volatile composition of Zhenjiang aromatic vinegar, one of the four famous China-style cereal vinegars, by using headspace solid-phase microextraction (HS-SPME)/gas chromatography-mass spectrum (GC-MS) and chemometrics. For this purpose, the HS-SPME sampling method for the volatile compounds of Zhenjiang aromatic vinegar was optimized by a second-order rotatable central composite experimental design (CCD). A HS extraction of the volatile compounds by incubation on a 65 y,m thickness polydimethylsiloxane/divinylbenzene (PDMS/DVB) fibre during 44.2 min at 69.5℃ with 1.9g NaCI add gave the most effective and accurate extraction. By the optimized method, a total of 58 volatile compounds, including 9 alcohols, 13 acids, 16 esters, 5 aldehydes, 4 ketones and 8 heterocycle compounds, were identified from 13 aromatic vinegar samples manufactured in Zhenjiang region. By principal components analysis (PCA), the thirteen vinegar samples were classified into 3 groups, and 10 volatile compounds were chosen as characteristic compounds of Zhenjiang aromatic vinegars.
机译：这项研究的主要目的是通过使用顶空固相微萃取（HS-SPME）/气相色谱-质谱（GC-MS）测定镇江芳香醋的挥发性成分，这是中国四种著名的谷物醋之一。 ）和化学计量学。为此，通过二次可旋转中心复合实验设计（CCD）优化了镇江香醋挥发性化合物的HS-SPME采样方法。在添加了1.9 g NaCl的69.5℃下于65y，m厚的聚二甲基硅氧烷/二乙烯基苯（PDMS / DVB）纤维上温育44.2分钟，在HS上萃取挥发性化合物的方法最有效，最准确。通过优化方法，从镇江地区生产的13种香醋样品中鉴定出58种挥发性化合物，包括9种醇，13种酸，16种酯，5种醛，4种酮和8种杂环化合物。通过主成分分析（PCA），将13个食醋样品分为3组，选择10种挥发性化合物作为镇江香醋的特征化合物。

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  • 来源
    《Journal of the Institute of Brewing》 |2012年第1期|p.133-141|共9页
  • 作者

    Yong-Jian Yu; Zhen-Ming Lu; Ning-Hua Yu; Wei Xu; Guo-Quan Li; Jing-Song Shi; Zheng-Hong Xu;

  • 作者单位

    Laboratory of Pharmaceutical Engineering, School of Medicine and Pharmaceutics, Jiangnan University, Wuxi214122, P R China;

    Laboratory of Pharmaceutical Engineering, School of Medicine and Pharmaceutics, Jiangnan University, Wuxi214122, P R China;

    Laboratory of Pharmaceutical Engineering, School of Medicine and Pharmaceutics, Jiangnan University, Wuxi214122, P R China;

    Laboratory of Pharmaceutical Engineering, School of Medicine and Pharmaceutics, Jiangnan University, Wuxi214122, P R China;

    Jiangsu Hengshun Vinegar Industry Co., Ltd., Zhenjiang212043, P R China;

    Laboratory of Bioactive Products Process Engineering, School of Medicine and Pharmaceutics, Jiangnan University, Wuxi214122, P R China;

    State Key Laboratory of Food Science and Technology, Jiangnan University, Wuxi214122, PR China,Laboratory of Pharmaceutical Engineering, School of Medicine and Pharmaceutics, Jiangnan University, Wuxi214122, P R China;

  • 收录信息 美国《科学引文索引》(SCI);
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    headspace solid-phase microextraction (HS-SPME); gas chromatography-mass spectrum (GC-MS); principal component; analysis (PCA); volatile; zhenjiang aromatic vinegar;

    机译：顶空固相微萃取（HS-SPME）;气相色谱-质谱（GC-MS）;主成分分析（PCA）;易挥发镇江香醋;

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