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首页> 外文期刊>The Journal of the Textile Institute >Interaction between effects of ambient parameters and those of other important parameters on electrospinning of PEI/NMP solution
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Interaction between effects of ambient parameters and those of other important parameters on electrospinning of PEI/NMP solution

机译:PEI / NMP溶液电纺中环境参数与其他重要参数的相互作用

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摘要

By electrospinning method, fibers are produced with diameters ranging from hundred nanometers up to a few micrometers. In this study, the influence of ambient temperature and relative humidity on the morphology of electrospun polyetherimide (PEI) fibers at varying electrospinning parameters such as solution concentration, applied voltage, and tip-to-collector distance was investigated. 1-methyl-2-pyrrolidinone was used as a solvent for PEI. Morphology and diameter of electrospun PEI fibers were examined by field-emission scanning electron microscopy. It was seen that 20 wt% of the PEI solution shows the most increase in average diameters from 30 to 70% RH at 15, 25, and 35 ℃. It was also seen that 20 wt% of the PEI solution shows the most decrease in average diameters from 15 to 35 ℃ at each of the RH values. An interesting result was observed for 12 cm of tip-to-collector distance. The average fiber diameters firstly decreased from 15 to 25 ℃, and then increased from 25 to 35 ℃ for all of the RH values.
机译:通过静电纺丝法,可以生产直径范围从几百纳米到几微米的纤维。在这项研究中,研究了环境温度和相对湿度对电纺聚醚酰亚胺(PEI)纤维在不同电纺参数(例如溶液浓度,施加电压和吸头到集电极距离)的形貌的影响。 1-甲基-2-吡咯烷酮用作PEI的溶剂。通过场发射扫描电子显微镜检查了电纺PEI纤维的形貌和直径。可以看出,PEI溶液的20 wt%在15、25和35℃时,平均直径从30%RH增加到70%RH最多。还可以看出,在每个RH值下,PEI溶液的20 wt%的平均直径从15到35℃减小最多。吸头到收集器的距离为12 cm,观察到一个有趣的结果。对于所有RH值,平均纤维直径首先从15℃降低到25℃,然后从25℃增加到35℃。

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