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首页> 外文期刊>Materials science & engineering >Role of heat on the development of electrochemical sensors on bare and modified Co_3O_4/CuO composite nanopowder carbon paste electrodes
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Role of heat on the development of electrochemical sensors on bare and modified Co_3O_4/CuO composite nanopowder carbon paste electrodes

机译:热量对裸露和修饰的Co_3O_4 / CuO复合纳米粉碳糊电极上电化学传感器的开发的作用

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摘要

The Co_3O_4/CuO composite nanopowder (NP) was synthesized by a mechanochemical method and characterized by using powder X-ray diffraction (PXRD), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM) and energy-dispersive spectroscopy (EDS). The synthesized Co_3O_4/CuO NP was used as a modified carbon paste electrode (MCPE) and further the bare carbon paste and Co_3O_4/CuO NP modified carbon paste was heated at different temperatures (100, 150, 200 and 250 ℃) for 10 min. The Co_3O_4/CuO NP MCPE was used to study the consequences of scan rate and dopamine concentration. Furthermore the preheated modified electrodes were used to study the electrochemical response to dopamine (DA), ascorbic acid (AA) and uric acid (UA).
机译:采用机械化学方法合成了Co_3O_4 / CuO复合纳米粉(NP),并利用粉末X射线衍射(PXRD),傅立叶变换红外光谱(FTIR),扫描电子显微镜(SEM)和能量分散光谱(EDS)对其进行了表征。 。将合成的Co_3O_4 / CuO NP用作改性碳糊电极(MCPE),然后将裸碳糊和Co_3O_4 / CuO NP改性碳糊在不同温度(100、150、200和250℃)下加热10分钟。 Co_3O_4 / CuO NP MCPE用于研究扫描速率和多巴胺浓度的后果。此外,使用预热的修饰电极来研究对多巴胺(DA),抗坏血酸(AA)和尿酸(UA)的电化学响应。

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