Electrodeposition of Copper Indium Sulfide Films From Organic Solutions

Arif Raza; Robert Engelken; Brandon Kemp; Imran Khan; Wasim Aleem; Chris Barber

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Electrodeposition of Copper Indium Sulfide Films From Organic Solutions

机译：有机溶液电沉积硫化铜铟薄膜

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We report on organic solutions of CuCl_2, InCl_3, and elemental sulfur for electrodepositing CuIn_xS_y films. CuInS_2 and CuInSe_2 are promising solar cell materials; our work on CuInS_2 prefaces planned work on plating CuInSe_2 from nonaque-ous solvents. Two promising solvent systems are (1) mixed propylene carbonate and water and (2) mixed ethylene glycol, propionic acid, and water (Engelken et al., 1988). Gray-brown films of CuIn_xS_y (nominally CuInS_2) have been plated from both baths. Major problems include (1) reduction of Cu~(+2) to Cu and Cu_xS by the solvent at high temperatures (T > 100℃), hence depleting Cu~(+2), (2) poor adherence/uniformity, (3) controlling stoichiometry, and (4) sluggish indium deposition. The paper will discuss our routes to solving these problems and present film data.

机译：我们报告了用于电沉积CuIn_xS_y膜的有机溶液CuCl_2，InCl_3和元素硫。 CuInS_2和CuInSe_2是有前途的太阳能电池材料。我们在CuInS_2上的工作是在非水溶剂中电镀CuInSe_2的计划工作。两种有前途的溶剂系统是（1）混合碳酸亚丙酯和水，以及（2）混合乙二醇，丙酸和水（Engelken等，1988）。在两个镀液中均镀有CuIn_xS_y灰褐色薄膜（名义上为CuInS_2）。主要问题包括（1）在高温（T> 100℃）下溶剂将Cu〜（+2）还原为Cu和Cu_xS，从而耗尽Cu〜（+2），（2）附着力/均匀性差，（3 ）控制化学计量，以及（4）缓慢的铟沉积。本文将讨论我们解决这些问题的途径并介绍电影数据。

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《Proceedings of the Arkansas Academy of Science》 |1996年第1996期|p.99-104|共6页
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Arif Raza; Robert Engelken; Brandon Kemp; Imran Khan; Wasim Aleem; Chris Barber;
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3. A hybrid ink of binary copper sulfide nanoparticles and indium precursor solution for a dense CuInSe2 absorber thin film and its photovoltaic performance [J] . Ara Cho, SeJin Ahn, Jae Ho Yun Journal of Materials Chemistry: An Interdisciplinary Journal dealing with Synthesis, Structures, Properties and Applications of Materials, Particulary Those Associated with Advanced Technology . 2012,第34期

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Electrodeposition of Copper Indium Sulfide Films From Organic Solutions

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