SYNTHESIS AND STRUCTURAL CHARACTERIZATION OF THE NEW ARSENIC TELLURIDE RH4AS2TE4-CENTER-DOT(EN)

Dhingra SS.; Haushalter RC.; Warren CJ.

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SYNTHESIS AND STRUCTURAL CHARACTERIZATION OF THE NEW ARSENIC TELLURIDE RH4AS2TE4-CENTER-DOT(EN)

机译：新型碲化亚锡RH4AS2TE4-CENTER-DOT（EN）的合成及结构表征

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The ethylenediamine (en) extraction of an alloy of nominal composition Rb4As2Te4 and subsequent concentration of the solution gave Rb4As2Te4 .(en) (1) as dark red crystals in 40% yield. The single crystal X-ray diffraction data revealed a novel dimeric [As2Te4](4-) anion, which consists of an As-As bonded As-4(4+) dimer bonded to four Te atoms. Each of the As atoms are in a trigonal pyramidal coordination environment. (C) 1997 Elsevier Science Ltd. [References: 41]

机译：用乙二胺（en）萃取标称组成为Rb4As2Te4的合金，然后将溶液浓缩，得到Rb4As2Te4。（en）（1），为深红色晶体，收率为40％。单晶X射线衍射数据揭示了一种新型的二聚[As2Te4]（4-）阴离子，它由与四个Te原子键合的As-As键合的As-4（4+）二聚体组成。每个As原子都处于三角锥型配位环境中。（C）1997 Elsevier Science Ltd. [参考：41]

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《Polyhedron: The International Journal for Inorganic and Organometallic Chemistry》 |1997年第17期|共5页
作者
Dhingra SS.; Haushalter RC.; Warren CJ.;
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正文语种 eng
中图分类化学;无机化学;
关键词
Arsenic tellurides; Extraction of intermetallic phases; Crystal structure; Post-transition elements; One-dimensional chains; Te zintl anions; Electrochemical synthesis; Cathodic dissolution; Sb2te3 electrodes; Salt; Polyanions; Polymers; Compound;

机译：碲化砷;金属间相的萃取;晶体结构;过渡元素;一维链;Te zintl阴离子;电化学合成;阴极溶解;Sb2te3电极;盐;多阴离子;聚合物;化合物;

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SYNTHESIS AND STRUCTURAL CHARACTERIZATION OF THE NEW ARSENIC TELLURIDE RH4AS2TE4-CENTER-DOT(EN)

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