N-SALICYLIDENEAMINO-ACIDATE COMPLEXES OF OXOVANADIUM(IV) .2. SYNTHESIS, CHARACTERIZATION AND DEAMINATION OF AN N-SALICYLIDENEGLYCYLGLYCINATO COMPLEX

Cavaco I.; Luz SM.; Duarte MT.; Matias PM.; Henriques RT. Gillard RD.; Pessoa JC.

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N-SALICYLIDENEAMINO-ACIDATE COMPLEXES OF OXOVANADIUM(IV) .2. SYNTHESIS, CHARACTERIZATION AND DEAMINATION OF AN N-SALICYLIDENEGLYCYLGLYCINATO COMPLEX

机译：氧钒（IV）的N-水杨酸氨基络合物.2。 N-水杨基乙二醇基络合物的合成，表征和脱氨

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A vanadium(IV) complex VO(sal-glygly) (H2O)(n), (1) (sal-glygly = N-salicylideneglycylglycinate ; n = 1.5-3.0) has been isolated from relatively concentrated solutions containing oxovanadium(IV), glycylglycine and salicylaldehyde, and characterized by elemental analysis, thermal (TG and DSC), magnetic and spectroscopic techniques. From similar but dilute solutions the decavanadate, (NH4)(4)(Na)(2)[V10O28]. 10 H2O (2) was isolated after ageing: its structure has been determined by X-ray diffraction analysis. The NH4+ cations were formed by deamination of the glycylglycine present in solution. [References: 35]

机译：钒（IV）配合物VO（sal-glygly）（H2O）（n），（1）（sal-glygly = N-水杨亚基甘氨酸甘氨酸盐; n = 1.5-3.0）已从含有氧钒（IV）的相对浓缩的溶液中分离出来，甘油甘氨酸和水杨醛，并通过元素分析，热（TG和DSC），磁和光谱技术进行表征。用相似但稀的溶液制备十钒酸盐（NH4）（4）（Na）（2）[V10O28]。老化后分离出10 H2O（2）：其结构已通过X射线衍射分析确定。 NH4 +阳离子是通过将溶液中存在的甘氨酰甘氨酸脱氨基而形成的。 [参考：35]

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《Polyhedron: The International Journal for Inorganic and Organometallic Chemistry》 |1995年第3期|共11页
作者
Cavaco I.; Luz SM.; Duarte MT.; Matias PM.; Henriques RT. Gillard RD.; Pessoa JC.;
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正文语种 eng
中图分类化学;无机化学;
关键词
Oxidative deamination; Crystal-structure; Amino-acids; Decavanadates; Bases;

机译：氧化脱氨;晶体结构;氨基酸;十钒酸盐;碱;

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1. N-SALICYLIDENEAMINO-ACIDATE COMPLEXES OF OXOVANADIUM(IV) .2. SYNTHESIS, CHARACTERIZATION AND DEAMINATION OF AN N-SALICYLIDENEGLYCYLGLYCINATO COMPLEX [J] . Cavaco I., Luz SM., Duarte MT., Polyhedron: The International Journal for Inorganic and Organometallic Chemistry . 1995,第3期

机译：氧钒（IV）的N-水杨酸氨基络合物.2。 N-水杨基乙二醇基络合物的合成，表征和脱氨
2. Oxovanadium(IV) complexes of bioinorganic and medicinal relevance: Synthesis, characterization and 3D molecular modeling and analysis of some oxovanadium(IV) complexes involving the O,N-donor environment of pyrazolone-based sulfa drug Schiff bases [J] . Maurya RC, Rajput S Journal of Molecular Structure . 2006,第1a3期

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4. New Catalytic Polymeric Membranes Incorporating Ti(IV) Trialkanolamines Complexes: Synthesis, Characterization, and Application in Catalysis [C] . M. G. Buonomenna, E. Drioli, G. Licini, American Chemical Society National Meeting . 2005

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机译：生物无机和药用相关的氧钒（IV）配合物：涉及水杨醛基磺胺类药物schiff碱的O，N-供体环境的一些氧钒（IV）配合物的合成，表征和3D分子模拟

N-SALICYLIDENEAMINO-ACIDATE COMPLEXES OF OXOVANADIUM(IV) .2. SYNTHESIS, CHARACTERIZATION AND DEAMINATION OF AN N-SALICYLIDENEGLYCYLGLYCINATO COMPLEX

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