Analytical and regulatory aspects for determination of macrolide residues in animal-derived foods by liquid chromatography associated with mass spectrometry [ASPECTOS ANALíTICOS E REGULATóRIOS NA DETERMINA? ?O DE RESíDUOS DE MACROLíDEOS EM ALIMENTOS DE ORIGEM ANIMAL POR CROMATOGRAFIA LíQUIDA ASSOCIADA à ESPECTROMETRIA DE MASSAS]

Sismotto M.; Paschoal J.A.R.; Reyes F.G.R.

首页> 外文期刊>Quimica nova >Analytical and regulatory aspects for determination of macrolide residues in animal-derived foods by liquid chromatography associated with mass spectrometry [ASPECTOS ANALíTICOS E REGULATóRIOS NA DETERMINA? ?O DE RESíDUOS DE MACROLíDEOS EM ALIMENTOS DE ORIGEM ANIMAL POR CROMATOGRAFIA LíQUIDA ASSOCIADA à ESPECTROMETRIA DE MASSAS]

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Analytical and regulatory aspects for determination of macrolide residues in animal-derived foods by liquid chromatography associated with mass spectrometry [ASPECTOS ANALíTICOS E REGULATóRIOS NA DETERMINA? ?O DE RESíDUOS DE MACROLíDEOS EM ALIMENTOS DE ORIGEM ANIMAL POR CROMATOGRAFIA LíQUIDA ASSOCIADA à ESPECTROMETRIA DE MASSAS]

机译：质谱联用液相色谱法测定动物源性食品中大环内酯残留物的分析和法规规定[测定和分析方面？液相色谱法与质谱法联用分析动物源性食品中的宏观污染物]

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This is an overview of LC-MS techniques applied for macrolide determination in food, including sample preparation and method validation, as well as the policies adopted by international agencies regarding their presence in food. Techniques for the analysis of macrolides in food normally include solid phase or liquid-liquid extraction followed by HPLC. UHPLC presents advantages in running time, detectability and solvent consumption. Triple-quadrupoles are the most common analyzers in instruments used for the determination of contaminants in food, but time-of-flight and ion-trap spectrometers have been successfully applied for analyses focusing on the investigation of structural formula or the presence of degradation products.

机译：这是用于食品中大环内酯测定的LC-MS技术的概述，包括样品制备和方法验证，以及国际机构在食品中存在大环内酯时所采用的政策。分析食品中大环内酯类的技术通常包括固相萃取或液-液萃取，然后进行HPLC。 UHPLC在运行时间，可检测性和溶剂消耗方面均具有优势。三重四极杆是用于确定食品中污染物的仪器中最常见的分析仪，但飞行时间和离子阱光谱仪已成功用于分析，重点在于研究结构式或降解产物的存在。

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《Quimica nova》 |2013年第3期|共13页
作者
Sismotto M.; Paschoal J.A.R.; Reyes F.G.R.;
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原文格式 PDF
正文语种 por
中图分类 54;
关键词
Liquid chromatography; Macrolides; Mass spectrometry;

机译：液相色谱法;大卤化物;质谱法;

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1. Analytical and regulatory aspects for determination of macrolide residues in animal-derived foods by liquid chromatography associated with mass spectrometry [ASPECTOS ANALíTICOS E REGULATóRIOS NA DETERMINA? ?O DE RESíDUOS DE MACROLíDEOS EM ALIMENTOS DE ORIGEM ANIMAL POR CROMATOGRAFIA LíQUIDA ASSOCIADA à ESPECTROMETRIA DE MASSAS] [J] . Sismotto M., Paschoal J.A.R., Reyes F.G.R. Quimica nova . 2013,第3期

机译：质谱联用液相色谱法测定动物源性食品中大环内酯残留物的分析和法规规定[测定和分析方面？液相色谱法与质谱法联用分析动物源性食品中的宏观污染物]
2. Principais técnicas de preparo de amostra para a determina??o de resíduos de agrotóxicos em água por cromatografia líquida com detec??o por arranjo de diodos e por espectrometria de massas [J] . Ednei Gilberto Primel, Fábio Ferreira Gon?alves, Manoel Leonardo Martins, Química Nova . 2011,第9期

机译：液相色谱-二极管阵列检测-质谱法测定水中农药残留的主要样品制备技术
3. Analytical and regulatory aspects for determination of macrolide residues in animal-derived foods by liquid chromatography associated with mass spectrometry [J] . Paschoal Jonas Augusto Rizzato, Reyes Felix G. R., Sismotto Marcela, Quimica nova . 2013,第3期

机译：质谱联用液相色谱法测定动物源性食品中大环内酯残留的分析和监管方面
4. LARGE SCALE MULTI-RESIDUE METHODSBY GAS AND LIQUID CHROMATOGRAPHY-MASS SPECTROMETRY FOR THE DETERMINATION OF PESTICIDE RESIDUES IN FOOD MATRICES [C] . Botitsi Eleni, Antoniou Spyros, Tsipi Despina IMEKOFOODS Conference . 2018

机译：气体和液相色谱 - 质谱法测定食品基质中农药残留量的大规模多残基方法
5. Multiresidue determination of pesticides in lettuce, tomatoes and celery by gas chromatography/chemical ionization/ion trap/mass spectrometry and liquid chromatography/atmospheric pressure chemical ionization/mass spectrometry. [D] . Jin, Baoping. 1999

机译：通过气相色谱/化学电离/离子阱/质谱和液相色谱/大气压化学电离/质谱法对生菜，西红柿和芹菜中的农药进行多残留测定。
6. A modified QuEChERS method coupled with liquid chromatography-tandem mass spectrometry for the simultaneous detection and quantification of scopolamine L-hyoscyamine and sparteine residues in animal-derived food products [O] . Weijia Zheng, Kyung-Hee Yoo, Jeong-Min Choi, 2019

机译：改进的QuEChERS方法与液相色谱-串联质谱联用可同时检测和定量动物源食品中东pol碱L-hycycyamine和sparteine残留
7. Analytical And Regulatory Aspects For Determination Of Macrolide Residues In Animal-derived Foods By Liquid Chromatography Associated With Mass Spectrometry [aspectos AnalÍticos E RegulatÓrios Na DeterminaÇ Ão De ResÍduos De MacrolÍdeos Em Alimentos De Origem Animal Por Cromatografia LÍquida Associada À Espectrometria De Massas] [O] . Sismotto M., Paschoal J.A.R., Reyes F.G.R. 2015

机译：质谱联用测定动物源性食品中大环内酯残留的分析和监管方面
8. Determinazione dell'acido S-fenilmercapturico mediante cromatografia liquida accoppiata a spettrometria di massa con trappola ionica (S-phenylmercapturic Acid Determination through Liquid Chromatography and Mass Spectrometry with Ion Trap). [R] . La Rocca, C., Baldassarri, L. T., Casella, M. L. 2002

机译：Resminazione dell'acido s-fenilmercapturico mediante cromatografia liquida accoppiata a spettrometria di massa con trappola ionica（通过液相色谱法和离子阱质谱法测定s-苯基巯基尿酸）。

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