Sonochemical synthesis of a new nano-structures bismuth(III) supramolecular compound: New precursor for the preparation of bismuth(III) oxide nano-rods and bismuth(III) iodide nano-wires

Nilofar Soltanzadeh; Ali Morsali

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Sonochemical synthesis of a new nano-structures bismuth(III) supramolecular compound: New precursor for the preparation of bismuth(III) oxide nano-rods and bismuth(III) iodide nano-wires

机译：声化学合成新型纳米结构超分子铋（III）：制备氧化铋（III）纳米棒和碘化铋（III）纳米线的新前体

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A new nanostructured Bi(III) supramolecular compound, {[Bi2(4,40-Hbipy)1.678(4,40-Hbipy)0.322(l-I)2I5.678](4,40-bipy)} (1), 4,40-bipy = 4,40-bipyridine} was synthesized by a sonochemical method. The nano-structure of 1 was investigated using scanning electron microscopy, powder X-ray powder diffraction (XRD),IR spectroscopy and elemental analysis, and the crystal structure of compound 1 was determined by single-crystal X-ray diffraction. The thermal stability of bulk compound 1 and of nano sized particles was studied by thermal gravimetric (TG) and differential thermal analyses (DTA). Bi2O3 and BiI3 nano-structures were obtained by calcinations of nano-structures of compound 1 at 400 C under air and nitrogen atmospheres,respectively.

机译：一种新型的纳米结构Bi（III）超分子化合物{[Bi2（4,40-Hbipy）1.678（4,40-Hbipy）0.322（II）2I5.678]（4,40-bipy）}（1），4，通过声化学方法合成了40-联吡啶＝ 4,40-联吡啶}。使用扫描电子显微镜，粉末X射线粉末衍射（XRD），红外光谱和元素分析研究了1的纳米结构，并通过单晶X射线衍射确定了化合物1的晶体结构。通过热重分析（TG）和差热分析（DTA）研究了本体化合物1和纳米颗粒的热稳定性。通过分别在空气和氮气气氛下在400℃下煅烧化合物1的纳米结构获得Bi 2 O 3和BiI 3纳米结构。

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《Ultrasonics sonochemistry》 |2010年第1期|共6页
作者
Nilofar Soltanzadeh; Ali Morsali;
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正文语种 eng
中图分类超声化学;
关键词
Nano-structure; Supramolecular; Bismuth(III); Crystal structure;

机译：纳米结构;超分子;铋（III）;晶体结构;

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1. Sonochemical synthesis of a new nano-structures bismuth(III) supramolecular compound: New precursor for the preparation of bismuth(III) oxide nano-rods and bismuth(III) iodide nano-wires [J] . Nilofar Soltanzadeh, Ali Morsali Ultrasonics sonochemistry . 2010,第1期

机译：声化学合成新型纳米结构超分子铋（III）：制备氧化铋（III）纳米棒和碘化铋（III）纳米线的新前体
2. Sonochemical Synthesis of Bismuth(III) Nano Coordination Compound and Direct Synthesis of Bi2O3 Nanoparticles from a Bismuth(III) Nano Coordination Compound Precursor [J] . Roodsari Majid Sadeghi, Shaabani Behrouz, Mirtamizdoust Babak, Journal of inorganic and organometallic polymers and materials . 2015,第5期

机译：铋（III）纳米配位化合物的声化学合成和铋（III）纳米配位化合物前体的直接合成Bi2O3纳米颗粒
3. Syntheses and characterization of a new nano-structured bismuth(III) bromide coordination polymer; new precursor for preparation of bismuth(III) bromide and bismuth(III) oxide nanostructures [J] . NILOFAR SOLTANZADEH, ALI MORSALI Journal of Coordination Chemistry . 2009,第17期

机译：新型纳米结构溴化铋（III）配位聚合物的合成与表征用于制备溴化铋（III）和氧化铋（III）纳米结构的新前体
4. Bismuth Compounds for Medicine: Synthesis of Bismuth (III) Subgallate Trihydrate [C] . O. A. Logutenko, Y. M. Yukhin, V. I. Evseenko International Forum on Strategic Technology . 2008

机译：医学铋化合物：铋（III）的合成 - 氨基铵三水合物
5. I. Multicatalysis: Development of a Bismuth(III) triflate-catalyzed Nucleophilic addition/ Hydrofunctionalization Reaction in the Synthesis of Complex Heterocycles II. C--H Arylation of Arenes and Heteroarenes with Palladium-Carboxylate Catalysts: Identification of the Catalyst Resting State and the Crucial Role of Pivalate Ligand in Stabilization of the Catalyst III. C--H Arylation of Heteroarenes with Palladium-Carboxylate Catalysts: Importance of Phosphine Ligand for Basic Heteroarene Substrates IV. C--H Arylation of Heteroarenes with Palladium-Carboxylate Catalysts: Effect of the Properties of Basic Heteroarene Substrates on Direct Arylations. [D] . Tundel, Rachel E. 2011

机译：I.多催化作用：在复杂的杂环化合物的合成中三氟甲磺酸铋（III）催化的亲核加成/加氢官能化反应的发展。羰基钯催化剂对芳烃和杂芳烃的CH-H芳基化反应：催化剂静止状态的鉴定以及新戊酸酯配体在稳定催化剂中的关键作用III。羰基钯催化剂催化杂芳烃的CH芳基化：膦配体对基础杂芳烃基质的重要性IV。杂芳烃与钯-羧酸酯的CH芳基化：碱性杂芳烃底物性能对直接芳基化的影响。
6. Improved Antileishmanial Activity of Dppz through Complexation with Antimony(III) and Bismuth(III): Investigation of the Role of the Metal [O] . Edgar H. Lizarazo-Jaimes, Rubens L. Monte-Neto, Priscila G. Reis, 2012

机译：通过与锑（III）和铋（III）络合提高Dppz的抗leishmanial活性：金属的作用研究
7. Environmentally Friendly Organic Synthesis Using Bismuth Compounds: Bismuth(III) Iodide Catalyzed Deprotection of Acetals in Water [O] . Mohan, Ram, Bailey, Aaron, Baru, Ashvin, 2008

机译：使用铋化合物的环境友好的有机合成：碘化铋（III）催化乙缩醛在水中的脱保护

Sonochemical synthesis of a new nano-structures bismuth(III) supramolecular compound: New precursor for the preparation of bismuth(III) oxide nano-rods and bismuth(III) iodide nano-wires

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