A Synthetic Method for Transition-Metal Chalcogenide Nanocrystals

Wang DS; Zheng W; Hao CH; Peng Q; Li YD

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A Synthetic Method for Transition-Metal Chalcogenide Nanocrystals

机译：过渡金属硫属化物纳米晶的合成方法

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In this paper, we prepared a series of chalcogenide semiconductor nanocrystals in controllable shape and size via a facile wet route using metal nitrates and sulfur or selenium powder as precursors and octadecylamine (ODA) as solvent. The as-obtained chalcogenides included CdS, MnS, Ag2S, PbS, Cu1.8S, Bi2S3, ZnS, ZnxCd1-xS, as well as Ag2Se, Cu2-xSe, CdSe. MnSe. Furthermore. these cyclohexane-soluble monodisperse nanocrystals were assembled to water-soluble colloidal spheres and the adjustment of assembly orderliness has been achieved by controlling the experimental parameters. The general synthesis and assembly of chalcogenide semiconductors provide ideal building blocks for various potential applications.

机译：在本文中，我们以金属硝酸盐和硫或硒粉为前体，以十八烷基胺（ODA）为溶剂，通过简便的湿法制备了一系列形状和尺寸可控的硫族化物半导体纳米晶体。所获得的硫族化物包括CdS，MnS，Ag2S，PbS，Cu1.8S，Bi2S3，ZnS，ZnxCd1-xS以及Ag2Se，Cu2-xSe，CdSe。锰硒此外。将这些可溶于环己烷的单分散纳米晶体组装成水溶性胶体球，并通过控制实验参数实现了组装有序性的调节。硫族化物半导体的一般合成和组装为各种潜在应用提供了理想的基础。

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《Chemistry: A European journal》 |2009年第8期|共6页
作者
Wang DS; Zheng W; Hao CH; Peng Q; Li YD;
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正文语种 eng
中图分类化学;
关键词
chalcogens; colloids; nanostructures; semiconductors; transition metals; NANOWIRE BUILDING-BLOCKS; QUANTUM DOTS; SEMICONDUCTOR NANOCRYSTALS; ROOM-TEMPERATURE; SULFIDE; MONODISPERSE; GROWTH; PRECURSORS; AG2SE; CDSE;

机译：硫族元素;胶体;纳米结构;半导体;过渡金属;纳米建筑砌块;量子点;半导电纳米晶;室温;硫化物;单晶;生长;PRASERSORS;AG2SE;CDSE;

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1. A Synthetic Method for Transition-Metal Chalcogenide Nanocrystals [J] . Wang DS, Zheng W, Hao CH, Chemistry: A European journal . 2009,第8期

机译：过渡金属硫属化物纳米晶的合成方法
2. Chemical Synthetic Strategy for Single-Layer Transition-Metal Chalcogenides [J] . Dongwon Yoo, Minkyoung Kim, Sohee Jeong, Journal of the American Chemical Society . 2014,第42期

机译：单层过渡金属硫属化物的化学合成策略
3. Synthetic, structural, NMR, and computational study of a geminally bis(peri-substituted) tridentate phosphine and its chalcogenides and transition-metal complexes [J] . Ray M.J., Randall R.A.M., Arachchige K.S.A., Inorganic Chemistry: A Research Journal that Includes Bioinorganic, Catalytic, Organometallic, Solid-State, and Synthetic Chemistry and Reaction Dynamics . 2013,第8期

机译：双（双取代）三齿膦及其硫族化物和过渡金属配合物的合成，结构，NMR和计算研究
4. Multi-Photon Absorption in Monolayer Transition-Metal Di-Chalcogenides and its Applications for Sub-band Multi-Photon Detection [C] . Feng Zhou, Wei Ji Conference on Lasers and Electro-Optics Pacific Rim . 2018

机译：单层过渡金属二硫胺基化物中的多光子吸收及其用于子带多光子检测的应用
5. Nanoscale Engineering of Transition-Metal Chalcogenides/Hydroxides for Boosting Electrochemical Energy Storage. [D] . Chen, Gen. 2016

机译：过渡金属硫属元素化物/氢氧化物的纳米级工程技术，可增强电化学储能。
6. Role of Crystal Structure and Chalcogenide Redox Properties on the Oxidative Assembly of Cadmium Chalcogenide Nanocrystals [O] . Jessica L. Davis, Aaron M. Chalifoux, Stephanie L. Brock -1

机译：晶体结构和硫族化物氧化还原特性在镉硫族化物纳米晶体氧化组装中的作用
7. Soft-Chemical Method for Synthesizing Intermetallic Antimonide Nanocrystals from Ternary Chalcogenide [O] . -1

机译：从三元硫属化物中合成金属间锑苷酸纳米晶体的软化物方法

A Synthetic Method for Transition-Metal Chalcogenide Nanocrystals

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