Reliable and diverse synthesis of aryl azides through copper-catalyzed coupling of boronic acids or esters with TMSN_3

Li Y.; Gao L.-X.; Han F.-S.

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Reliable and diverse synthesis of aryl azides through copper-catalyzed coupling of boronic acids or esters with TMSN_3

机译：通过铜催化硼酸或酯与TMSN_3的偶联可靠可靠地合成芳基叠氮化物

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摘要

(Figure Presented) Aryl azide formation: The copper-catalyzed coupling reaction of boronic esters and acids with TMSN_3 have been presented as a highly efficient, simple, broadly applicable, and less hazardous methodology for the practi cal synthesis of aryl azides with structural diversity (see scheme).

机译：（显示的图）芳基叠氮化物的形成：硼酸酯和酸与TMSN_3的铜催化偶联反应已被证明是一种高效，简单，适用范围广且危害较小的方法，用于实际合成具有结构多样性的芳基叠氮化物（参见方案）。

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《Chemistry: A European journal》 |2010年第27期|共4页
作者
Li Y.; Gao L.-X.; Han F.-S.;
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正文语种 eng
中图分类应用化学;
关键词
Aryl azides; Boronic acids; Boronic esters; Copper; Cross-coupling;

机译：芳基叠氮化物;硼酸;硼酸酯;铜;交叉偶联;

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专利

1. Reliable and diverse synthesis of aryl azides through copper-catalyzed coupling of boronic acids or esters with TMSN_3 [J] . Li Y., Gao L.-X., Han F.-S. Chemistry: A European journal . 2010,第27期

机译：通过铜催化硼酸或酯与TMSN_3的偶联可靠可靠地合成芳基叠氮化物
2. Copper-catalyzed synthesis of aryl azides and 1-aryl-1,2,3-triazoles from boronic acids [J] . Chuan-Zhou Tao, Xin Cui, Juan Li Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2007,第20期

机译：铜催化硼酸合成芳基叠氮化物和1-芳基-1,2,3-三唑
3. Metal-free synthesis of aryl esters by coupling aryl carboxylic acids and aryl boronic acids [J] . Jayaraman Sembian Ruso, Nagappan Rajendiran, Rajendran Senthil Kumaran Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2014,第15期

机译：通过偶合芳基羧酸和芳基硼酸的无金属合成芳基酯
4. Micro-reactor synthesis: synthesis of cyanobiphenyls using a modified suzuki coupling of an aryl halide and aryl boronic acid. [C] . Victoria Skelton, Gillian M.Greenway, Stephen J.Haswell, International conference on microreaction technology . 2000

机译：微反应器合成：使用芳基卤化物和芳族硼酸的改性铃木偶联来合成氰基苯基。
5. Ambient temperature synthesis of high enantiopurity N-protected peptidyl ketone by desulfitative cross coupling of peptidyl thiol esters and boronic acids [D] . Yang, Hao 2009

机译：肽基硫醇酯与硼酸的脱硫交叉偶联在环境温度下合成高对映纯度的N-保护的肽基酮
6. Palladium-Catalyzed Direct Boronic Acid Synthesis from Aryl Chlorides: A Simplified Route to Diverse Boronate Ester Derivatives [O] . Gary A. Molander, Sarah L.J. Trice, Spencer D. Dreher -1

机译：钯催化直接硼酸合成从芳基氯化物：简化路由到多元硼酸酯衍生物
7. Easy Copper-Catalyzed Synthesis of Primary Aromatic Amines by Coupling Aromatic Boronic Acids with Aqueous Ammonia at Room Temperature [O] . Rao H. H., Fu H., Jiang Y. Y., 2009

机译：室温下将芳族硼酸与氨水偶联容易的铜催化合成伯胺

Reliable and diverse synthesis of aryl azides through copper-catalyzed coupling of boronic acids or esters with TMSN_3

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