Adamantylation of Pyridine Derivatives

Shadrikova V. A.; Golovin E. V.; Klimochkin Yu. N.

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Adamantylation of Pyridine Derivatives

机译：吡啶衍生物的金刚烷基化

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摘要

The reaction of isomeric hydroxypyridines with 1-bromoadamantane under various conditions led to mono- and disubstituted D-, D-, and N-adamantylation products. Hydroxypyridines and 4-dimethyl-aminopyridine were found to have catalytic effect on the quaternization of pyridine with adamantyl bromide. A method was developed for the preparation of quaternary 1-(adamant-1-yl)pyridinium salts under mild conditions.

机译：异构体羟基吡啶与1-溴金刚烷在各种条件下的反应产生单-和双取代的D-，D-和N-金刚烷基化产物。发现羟基吡啶和4-二甲基-氨基吡啶对金刚烷基溴对吡啶的季铵化有催化作用。开发了一种在温和条件下制备季铵1-（金刚烷基-1-基）吡啶鎓盐的方法。

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来源
《Chemistry of heterocyclic compounds》 |2015年第11期|共9页
作者
Shadrikova V. A.; Golovin E. V.; Klimochkin Yu. N.;
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正文语种 eng
中图分类杂环化合物;
关键词
1-(adamant-1-yl)pyridinium bromide; 1-bromoadamantane; 4-dimethylaminopyridine; hydroxypyridine; 1H-pyridone; adamantylation; alkylation; quaternization;

机译：1-（金刚烷-1-基）溴化吡啶;1-溴金刚烷;4-二甲基氨基吡啶;羟基吡啶;1H-吡啶酮;金刚烷基化;烷基化;季铵化;

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1. Adamantylation of Pyridine Derivatives [J] . Shadrikova V. A., Golovin E. V., Klimochkin Yu. N. Chemistry of heterocyclic compounds . 2015,第11期

机译：吡啶衍生物的金刚烷基化
2. Ion-exchange-resin-catalyzed adamantylation of phenol derivatives with adamantanols: Developing a clean process for synthesis of 2-(1-adamantyl)-4-bromophenol, a key intermediate of adapalene [J] . Nan Wang, Ronghua Wang, Xia Shi, Beilstein journal of organic chemistry. . 2012,第1期

机译：离子交换树脂催化的金刚烷醇与苯酚衍生物的金刚烷化：开发一种清洁的方法合成2-（1-金刚烷基）-4-溴苯酚，这是阿达帕林的关键中间体
3. Ion-exchange-resin-catalyzed adamantylation of phenol derivatives with adamantanols: Developing a clean process for synthesis of 2-(1-adamantyl)-4-bromophenol, a key intermediate of adapalene [J] . Nan Wang, Ronghua Wang, Xia Shi, Beilstein journal of organic chemistry. . 2012,第1期

机译：离子交换树脂催化的金刚烷醇与苯酚衍生物的金刚烷化：开发一种清洁的方法合成2-（1-金刚烷基）-4-溴苯酚，这是阿达帕林的关键中间体
4. Quenching efficacy of TiO_2 on novel pyridine derivative: A photophysical investigation [C] . Aishwarya Nadgir, Malatesh S. Pujar, Mahantesha Basanagouda, International Conference on Physics of Materials and Nanotechnology . 2020

机译：TiO_2对新型吡啶衍生物的猝灭功效：一种光物理调查
5. Bioremediation of subsurface sediment and groundwater contaminated with pyridine and pyridine derivatives. [D] . Ronen, Zeev. 1992

机译：吡啶和吡啶衍生物污染的地下沉积物和地下水的生物修复。
6. Ion-exchange-resin-catalyzed adamantylation of phenol derivatives with adamantanols: Developing a clean process for synthesis of 2-(1-adamantyl)-4-bromophenol a key intermediate of adapalene [O] . Nan Wang, Ronghua Wang, Xia Shi, 2012

机译：离子交换树脂催化的金刚烷醇与苯酚衍生物的金刚烷化：开发一种清洁的方法合成2-（1-金刚烷基）-4-溴苯酚这是阿达帕林的关键中间体
7. Ion-exchange-resin-catalyzed adamantylation of phenol derivatives with adamantanols: Developing a clean process for synthesis of 2-(1-adamantyl)-4-bromophenol, a key intermediate of adapalene [O] . Nan Wang, Ronghua Wang, Xia Shi, 2012

机译：离子交换树脂催化的金刚烷醇与苯酚衍生物的金刚烷化：开发一种清洁的方法合成2-（1-金刚烷基）-4-溴苯酚，这是阿达帕林的关键中间体

Adamantylation of Pyridine Derivatives

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